Type-B trichothecene calibrants: Comparison of HPLC and GC-results within an intercomparison study

Mycotoxin Research

Volumn 21, Issue 4, 2005, Pages 224-230

  Welzig, E ^a   Drs, E ^a   Josephs, R D ^b,c   Schothorst, R C ^d   Van Egmond, H P ^d   Pettersson, H ^e   Chan, D ^f   Krska, R ^a  

^a UNIVERSITY OF NATURAL RESOURCES AND LIFE SCIENCES   (Austria)

^b JOINT RESEARCH CENTRE   (Italy)

^c PAVILLON DE BRETEUIL   (France)

^d NATIONAL INSTITUTE FOR PUBLIC HEALTH AND THE ENVIRONMENT   (Netherlands)

^e SWEDISH UNIVERSITY OF AGRICULTURAL SCIENCES   (Sweden)

^f CENTRAL SCIENCE LABORATORY   (United Kingdom)

Author keywords

Calibrant; Deoxynivalenol; Gas chromatography; HPLC; Trichothecenes

Indexed keywords

EID: 33845774014     PISSN: 01787888     EISSN: 18671632     Source Type: Journal    
DOI: 10.1007/BF02957582     Document Type: Conference Paper

References (11)

1. Krska R, Welzig E, Josephs RD, Kandier W, Pettersson H, MacDonald S, Charlton A, Brereton P, Hametner C, Berner D, Zöllner P (2003) Purity assessment of crystalline zearalenone. Journal of AOAC Int 86(4):722-728
2. Krska R, Schothorst RC, Van Egmond HP, Josephs RD, Lepschy J, Pettersson H, Chan D, Berthiller F, Schuhmacher R, Kandier W, Welzig E (2005) Processing and Purity Assessment of Standards for the Analysis of Type-B Trichothecene Mycotoxins. Anal Bioanal Chem 382:1848-1858
3. Pettersson H, Langseth W (2002) Intercomparison of Trichothecene Analysis and Feasibility to Produce Certified Calibrants and Reference Material. Final report I, Homogeneity and Stability Studies, Final Intercomparison. BCR Information, EU Project Report EUR 20285/2 EN 1-145
4. Pettersson H, Langseth W (2002) Intercomparison of Trichothecene Analysis and Feasibility to Produce Certified Calibrants and Reference Material. Final report 1, Method Studies. BCR Information, Project Report EUR 20285/1 EN 1-82
5. IUPAC (1995) Pure Appl Chem 67:331-343
6. Davies PL (1988) Statistical evaluation of interlaboratory tests. Fresenius Z Anal Chem 331:513-519
7. Krska R, Baumgartner S, Josephs R (2001) The state-of-the-art in the analysis of type-A and-B trichothecene mycotoxins in cereals. Fresenius J Anal Chem 371:285-299
8. In: Horwitz W (ed) Official methods of analysis of the association of official analytical chemists, 17th Edition, Current through revision Arlington, USA, Method Nr. 986.17
9. In: Horwitz W (ed) Official methods of analysis of the association of official analytical chemists, 17th Edition, Current through revision Arlington, USA, Method Nr. 986.18
10. Trucksess MW, Page SW, Wood GE, Cho TH (1998) Determination of dexoynivalenol in white flour, whole wheat flour, and bran by solid phase extraction/liquid chromatography: interlaboratory study. Journal of AOAC Int 81:880-886
11. Thompson M (2000) Recent trends in interlaboratory precision at ppb and sub-ppb concentrations in relation to fitness for purpose criteria in proficiency testing. Analyst 125:385-386