An initial study on the formation of 3-MCPD esters during oil refining

European Journal of Lipid Science and Technology

Volumn 113, Issue 3, 2011, Pages 374-379

  Hrncirik, Karel ^a   van Duijn, Gerrit ^a  

^a UNILEVER RESEARCH VLAARDINGEN   (Netherlands)

Author keywords

3 MCPD ester; Chloropropanediols; Deodorization; Edible oils; Glycidyl ester

Indexed keywords

BRASSICA NAPUS;

EID: 79952592853     PISSN: 14387697     EISSN: 14389312     Source Type: Journal    
DOI: 10.1002/ejlt.201000317     Document Type: Article

References (15)

1. van Duijn, G., den Dekker, G., Unilever food safety assurance system for refined vegetable oils and fats. OCL 2010, 17, 100- 103.
2. van Duijn, G., Dumelin, E. E., Trautwein, E. A., in: Williams, C., Buttriss, J. (Eds.), Improving the Fat Content of Foods, Woodhead publishing Ltd., Cambridge, UK 2006, pp. 490- 507.
3. Velíšek, J., Davídek, J., Kubelka, V., Janícek, G. et al., New chlorine-containing organic compounds in protein hydrolysates. Agric. Food Chem. 1980, 28, 1142- 1144.
4. Gardner, A. M., Yurawecz, M. P., Cunningham, W. C., Diachenko, G. W. et al., Isolation and identification of C16 and C18 fatty acid esters of chloropropanediol in adulterated Spanish cooking oils. Bull. Environ. Contam. Toxicol. 1983, 31, 625- 630.
5. Svejkovská, B., Novotný, O., Divinová, V., Réblová, Z. et al., Esters of 3-chloropropane-1, 2-diol in foodstuffs. Czech. J. Food Sci. 2004, 22, 190- 196.
6. Divinová, V., Svejkovská, B., Novotný, O., Velíšek, J., Survey of 3-chloropropane-1, 2-diol and its precursors in foods in the Czech Republic. Czech. J. Food Sci. 2004, 22, 267- 271.
7. Zelinková, Z., Svejkovská, B., Velíšek, J., Doležal, M., Fatty acid esters of 3-chloropropane-1, 2-diol in edible oils. Food Addit. Contam. 2006, 23, 1290- 1298.
8. Weißhaar, R., Perz, R., Fatty acid esters of glycidol in refined fats and oils. Eur. J. Lipid Sci. Technol. 2010, 112, 158- 165.
9. Franke, K., Strijowski, U., Fleck, G., Pudel, F., Influence of chemical refining process and oil type on bound 3-chloro-1, 2-propanediol contents in palm oil and rapeseed oil. LWT-Food Sci. Technol. 2009, 42, 1751- 1754.
10. Weißhaar, R., Determination of total 3-chloropropane-1, 2-diol (3-MCPD) in edible oils by cleavage of MCPD esters with sodium methoxide. Eur. J. Lipid Sci. Technol. 2008, 110, 183- 186.
11. Hrncirik, K., Zelinková, Z., Ermacora, A., Critical factors of indirect determination of 3-chloropropane-1, 2-diol esters. Eur. J. Lipid Sci. Technol. 2011, 113, same issue.
12. Shimizu, M., Kudo, N., Shiro, H., Yasunga, K. et al., Comparison of indirect and direct quantification of glycidol fatty acid ester in edible oils. J. Oleo Sci. 2010, 59, 535- 539.
13. AOCS Official Method Ca 5a-40: Free fatty acids, in: Firestone, D. (Ed.), Official Methods and Recommended Practices of the AOCS, 6th Edn., AOCS, Champaign, IL, US 2009.
14. AOCS Official Method Cd 8b-90: Peroxide Value, in: Firestone, D. (Ed.), Official Methods and Recommended Practices of the AOCS, 6th Edn., AOCS, Champaign, IL, US 2009.
15. AOCS Official Method Cd 11b-91: Determination of Mono- and Diglycerides by Capillary Gas Chromatography, in: Firestone, D. (Ed.), Official Methods and Recommended Practices of the AOCS, 6th Edn., AOCS, Champaign, IL, US 2009.