Supercritical carbon dioxide extraction of marigold lutein fatty acid esters: Effects of cosolvents and saponification conditions

Separation Science and Technology

Volumn 46, Issue 4, 2011, Pages 605-610

  Palumpitag, Wisinee ^a   Prasitchoke, Phattanon ^b   Goto, Motonobu ^c   Shotipruk, Artiwan ^a  

^a CHULALONGKORN UNIVERSITY   (Thailand)

^b PTT   (Thailand)

^c KUMAMOTO UNIVERSITY   (Japan)

Author keywords

Cosolvent; Extraction; Lutein; Saponification; Xanthophylls

Indexed keywords

COSOLVENTS; FATTY ACID ESTERS; KOH SOLUTION; LUTEIN; MARIGOLD FLOWERS; OLIVE OIL; OPTIMAL CONDITIONS; PALM OIL; SOLUTION RATIO; SOYBEAN OIL; SUPERCRITICAL CARBON DIOXIDE EXTRACTION; SUPERCRITICAL CARBON DIOXIDES; XANTHOPHYLLS;

CARBON DIOXIDE; ESTERIFICATION; ESTERS; ETHANOL; FATTY ACIDS; POTASSIUM HYDROXIDE; RESINS; VEGETABLE OILS;

SUPERCRITICAL FLUID EXTRACTION;

EID: 79952417304     PISSN: 01496395     EISSN: 15205754     Source Type: Journal    
DOI: 10.1080/01496395.2010.533739     Document Type: Article

References (25)

1. Sowbhagya, H.B.; Sampathu, S.R.; Krishnamurthy, N. (2004) Natural colorant from marigold-chemistry and technology. Food Rev. Int., 20: 33-50.
2. Wang, M.; Tsao, R.; Zhang, S.; Dong, Z.; Yang, R.; Gong, J.; Pei, Y. (2006) Antioxidant activity, mutagenicity=anti-mutagenicity, and clastogenicity=anti-clastogenicity of lutein from marigold flowers. Food Chem. Toxicol., 44: 1522-1529.
3. Khachik, F. (1995) Process for isolation, purification, and recrystallization of lutein from saponified marigold oleoresin and uses thereof. United States Patent, 5382714.
4. Khachik, F. (2001) Process for extraction, purification of lutein, zeaxanthin and rare carotenoids from marigold flowers and plants. United States Patent, 6262284.
5. Ausich, R.; Sanders, D. (1997) Process for the formation, isolation, and purification of comestible xanthophylls crystals from plants. United States Patent, 5648564.
6. Roberta, P.; Marotti, M.; Grandi, S. (1998) Lutein and lutein ester content in different types of Tagetes patula and T. erecta. Ind. Crop Prod., 8: 45-51.
7. Deineka, V.I.; Sorokopudov, V.N.; Deineka, L.A.; Yu. Tret'yakovl, M. (2007) Flowers of marigold (Tagets) species as a source of xanthophylls. Pharma Chem. J., 41: 540-542.
8. Brunner, G. (2005) Supercritical fluids: Technology and application to food processing. J. Food Eng., 67: 21-33.
9. Katherine, L.S.; Edgar, C.; Jerry, W.; Luke Howard, R.; Julie, C. (2008) Extraction conditions affecting supercritical fluid extraction (SFE) of lycopene from watermelon. Bioresour. Technol., 99: 7835-7841.
10. Campos, L.M.A.S.; Michielin, E.M.Z.; Danielski, L.; Ferreira, S.R.S. (2005) Experimental data and modeling the supercritical fluid extraction of marigold (Calendula officinalis) oleoresin. J. Supercrit. Fluids, 34: 163-170.
11. Mattea, F.; Martin, A.; Cocero, J.S. (2009) Carotenoid processing with supercritical fluids. J. Food Eng., 93: 255-265.
12. Pereira, C.; Meireles, M.A.A. (2010) A supercritical fluid extraction of bioactive compounds: Fundamentals, applications and economic perspectives. Food Bioprocess Technol., 3: 340-372.
13. Ollanketo, M.; Hartonen, K.; Riekkola, M.L.; Holm, Y.; Hiltunen, R. (2001) Supercritical carbon dioxide extraction of lycopene in tomato skins. Eur. Food Res. Technol., 212: 561-565.
14. 2 fluid parameters on chemical composition and yield of carotenoids extracted from pumpkin. LWT-Food Sci. Technol., 43: 39-44.
15. 2 extraction of carotenoids from pitanga fruits (Eugenia uniflora L.). J. Supercrit. Fluids, 46: 33-39.
16. 2. J. Supercrit. Fluids, 44: 308-314.
17. 2 and the effect of solvent modifiers. J. Agric. Food Chem., 48: 5640-5642.
18. Krichnavaruk, S.; Shotipruk, A.; Goto, M.; Pavasant, P. (2008) Supercritical carbon dioxideextraction of astaxanthin from Haematococcus pluvialis with vegetable oils as co-solvent. Bioresour. Technol., 99: 5556-5560.
19. Sun, M.; Temelli, F. (2006) Supercritical carbon dioxide extraction of carotenoids from carrot using canola oil as a continuous co-solvent. J. Supercrit. Fluids, 37: 397-408.
20. Vasapollo, G.; Longo, L.; Rescio, L.; Ciurlia, L. (2004) Innovative supercritical CO2 extraction of lycopene from tomato in the presence of vegetable oil as co-solvent. J. Supercrit. Fluids, 29: 87-96.
21. Ma, Q.; Xu, X.; Gao, Y.; Wang, Q.; Zhao, J. (2008) Optimization of supercritical carbon dioxide extraction of lutein esters from marigold (Tagetes erecta L.) with soybean oil as a co-solvent. Int. J. Food Sci. Technol., 43: 1763-1769.
22. Horwitz, W. (Ed.). (2006) Official Methods of Analysis of AOAC International, Vol. 1, 18th Ed.; AOAC, AOAC International: Gaithersburg, MD.
23. 2 and composition profile. J. Chem Eng Process., 46: 99-106.
24. Ozlem, G.; Feral, T. (2005) Solubility behavior of ternary systems of lipids, cosolvents, and supercritical carbon dioxide and processing aspects. J. Supercrit. Fluids., 36: 1-15
25. Soares, B.M.C.; Gamarra, F.M.C.; Paviani, L.C.; Goncalves, L.A.G.; Cabral, F.A. (2007) Solubility of triacylglycerols in supercritical carbon dioxide. J. Supercrit. Fluids., 43: 25-31.