Improvement in HPLC separation of acetic acid and levulinic acid in the profiling of biomass hydrolysate

Bioresource Technology

Volumn 102, Issue 7, 2011, Pages 4938-4942

  Xie, Rui ^a   Tu, Maobing ^a   Wu, Yonnie ^a   Adhikari, Sushil ^b  

^a AUBURN UNIVERSITY   (United States)

^b AUBURN UNIVERSITY   (United States)

Author keywords

Acetic acid; Aminex column chromatography; Biomass; HPLC; Resolution

Indexed keywords

5 HYDROXYMETHYL FURFURALS; ACID CONCENTRATIONS; AMINEX COLUMN CHROMATOGRAPHY; BIOMASS HYDROLYSATES; CAPACITY FACTORS; COLUMN TEMPERATURE; HPLC; HPLC SEPARATION; LEVULINIC ACID; RESOLUTION;

ACETIC ACID; ALDEHYDES; BIOMASS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; METAL ANALYSIS; ORGANIC ACIDS; PH; SULFUR DETERMINATION; SULFURIC ACID;

COLUMN CHROMATOGRAPHY;

ACETIC ACID; LEVULINIC ACID; SULFURIC ACID;

ACETIC ACID; BIOMASS; LIQUID CHROMATOGRAPHY; SULFURIC ACID;

ARTICLE; BIOMASS; COLUMN CHROMATOGRAPHY; CONTROLLED STUDY; FLOW RATE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; SEPARATION TECHNIQUE; TEMPERATURE DEPENDENCE;

ACETIC ACID; BIOTECHNOLOGY; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; ETHANOL; LEVULINIC ACIDS; LIGNIN; SULFURIC ACIDS; TEMPERATURE;

EID: 79951960221     PISSN: 09608524     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.biortech.2011.01.050     Document Type: Article

References (15)

1. Alasandro M. Separation of diastereoisomers of DuP 105, a novel oxazolidinone antibacterial agent, by supercritical fluid chromatography on a Chiralcel OD column. J. Pharm. Biomed. Anal. 1996, 14(7):807-814.
2. Blake J.D., Clarke M.L., Richards G.N. Determination of organic-acids in sugarcane process juice by high-performance liquid-chromatography - improved resolution using dual Aminex HPX-87H cation-exchange columns equilibrated to different temperatures. J. Chromatogr. 1987, 398:265-277.
3. Calabro M.L., Raneri D., Tommasini S., Ficarra R., Alcaro S., Gallelli A., Micale N., Zappala M., Ficarra P. Enantio selective recognition of 2,3-benzodiazepin-4-one derivatives with anticonvulsant activity on several polysaccharide chiral stationary phases. J. Chromatogr. B 2006, 838(1):56-62.
4. Carrasco C., Baudel H.M., Sendelius J., Modig T., Roslander C., Galbe M., Hahn-Hagerdal B., Zacchi G., Liden G. SO2-catalyzed steam pretreatment and fermentation of enzymatically hydrolyzed sugarcane bagasse. Enzyme Microb. Technol. 2010, 46(2):64-73.
5. Cevasco G., Piatek A.M., Scapolla C., Thea S. An improved method for simultaneous analysis of aminothiols in human plasma by high-performance liquid chromatography with fluorescence detection. J. Chromatogr. A 2010, 1217(14):2158-2162.
6. Chen S.F., Mowery R.A., Castleberry V.A., van Walsum G.P., Chambliss C.K. High-performance liquid chromatography method for simultaneous determination of aliphatic acid, aromatic acid and neutral degradation products in biomass pretreatment hydrolysates. J. Chromatogr. A 2006, 1104(1-2):54-61.
7. Hu R.F., Lin L., Liu T.J., Liu S.J. Dilute sulfuric acid hydrolysis of sugar maple wood extract at atmospheric pressure. Bioresour. Technol. 2010, 101(10):3586-3594.
8. Larsson S., Palmqvist E., Hahn-Hagerdal B., Tengborg C., Stenberg K., Zacchi G., Nilvebrant N.O. The generation of fermentation inhibitors during dilute acid hydrolysis of softwood. Enzyme Microb. Technol. 1999, 24(3-4):151-159.
9. Palm M., Zacchi G. Extraction of hemicellulosic oligosaccharides from spruce using microwave oven or steam treatment. Biomacromolecules 2003, 4(3):617-623.
10. Pecina R., Bonn G., Burtscher E., Bobleter O. High-performance liquid-chromatographic elution behavior of alcohols, aldehydes, ketones, organic-acids and carbohydrates on a strong cation-exchange stationary phase. J. Chromatogr. 1984, 287(2):245-258.
11. Peter A., Peter M., Ilisz I., Fulop F. Comparison of column performances in direct high-performance liquid chromatographic enantioseparation of 1-or 3-methyl-substituted tetrahydroisoquinoline analogs. Application of direct and indirect methods. Biomed. Chromatogr. 2005, 19(6):459-465.
12. Ruiz, R., and Ehrman, T., 1996. Determination of carbohydrates in biomass by high performance liquid chromatography. In Chemical Analysis and Testing Task Laboratory Analytical Procedure LAP-002.
13. Scarlata C.J., Hyman D.A. Development and validation of a fast high pressure liquid chromatography method for the analysis of lignocellulosic biomass hydrolysis and fermentation products. J. Chromatogr. A 2010, 1217(14):2082-2087.
14. Snyder L.R., Kirkland J.J., Glajch J.L. Practical HPLC Method Development 1997, Wiley-Interscience, New York. second ed.
15. Srinivasan N., Ju L.K. Pretreatment of guayule biomass using supercritical carbon dioxide-based method. Bioresour. Technol. 2010, 101(24):9785-9791.