Development and validation of a fast high pressure liquid chromatography method for the analysis of lignocellulosic biomass hydrolysis and fermentation products

Journal of Chromatography A

Volumn 1217, Issue 14, 2010, Pages 2082-2087

  Scarlata, Christopher J ^a   Hyman, Deborah A ^a  

^a NATIONAL RENEWABLE ENERGY LABORATORY   (United States)

Author keywords

Acetic acid; Biomass; Cation exchange HPLC; Ethanol; Fast acid method; Furfural; Renewable energy

Indexed keywords

CATION EXCHANGES; CATION-EXCHANGE HPLC; FAST ACID METHOD; RENEWABLE ENERGIES; RENEWABLE ENERGY;

ACETIC ACID; ALDEHYDES; BIOMASS; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; ETHANOL; FURFURAL; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIQUIDS; METAL ANALYSIS; METHANOL; ORGANIC ACIDS; ORGANIC POLYMERS; PH EFFECTS; POSITIVE IONS; REFRACTIVE INDEX; RESINS;

HIGH PRESSURE LIQUID CHROMATOGRAPHY;

5 HYDROXYMETHYLFURFURAL; ACETIC ACID; ALCOHOL; ALCOHOL DERIVATIVE; CARBOXYLIC ACID; FUEL; FURAN DERIVATIVE; FURFURAL; LIGNOCELLULOSE;

ACCURACY; ARTICLE; BIOMASS CONVERSION; CHEMICAL ANALYSIS; CONTROLLED STUDY; FERMENTATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROLYSIS; ION EXCHANGE CHROMATOGRAPHY; PRIORITY JOURNAL; SENSITIVITY AND SPECIFICITY; VALIDATION PROCESS;

ACETIC ACID; BIOMASS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CHROMATOGRAPHY, ION EXCHANGE; ETHANOL; FERMENTATION; FURALDEHYDE; HYDROLYSIS; LIGNIN; LINEAR MODELS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY;

EID: 77649337271     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.01.061     Document Type: Article

References (25)

1. Himmel M.E., Ding S.Y., Johnson D.K., Adney W.S., Nimlos M.R., Brady J.W., and Foust T.D. Science 315 (2007) 804
2. A.D. Sluiter, B.R. Hames, R.O. Ruiz, C.J. Scarlata, J.B. Sluiter, D.W. Templeton, in: NREL Laboratory Analytical Procedures, U.S. Department of Energy, Golden, 2005.
3. Mohagheghi A., Ruth M., and Schell D.J. Process Biochem. 41 (2006) 1806
4. Wyman C.E., Dale B.E., Elander R.T., Holtzapple M., Ladisch M.R., and Lee Y.Y. Bioresour. Technol. 96 (2005) 1959
5. Pecina R., Bonn G., Burtscher E., and Bobleter O. J. Chromatogr. 287 (1984) 245
6. Huck C.W., Huber C.G., and Bonn G.K. In: El Rassi Z. (Ed). Journal of Chromatography Library vol. 66 (2002), Elsevier Science [Imprint] Elsevier Science & Technology Books, San Diego p. 1256
7. Bonn G., and Bobleter O. Chromatographia 18 (1984) 445
8. Dien B.S., Nagle N., Hicks K.B., Singh V., Moreau R.A., Tucker M.P., Nichols N.N., Johnston D.B., Cotta M.A., Nguyen Q., and Bothast R.J. Appl. Biochem. Biotechnol. 113-116 (2004) 937
9. Tucker M.P., Kim K.H., Newman M.M., and Nguyen Q.A. Appl. Biochem. Biotechnol. 105 (2003) 165
10. Nguyen Q.A., Tucker M.P., Keller F.A., and Eddy F.P. Appl. Biochem. Biotechnol. 84-86 (2000) 561
11. Nguyen Q.A., Dickow J.H., Duff B.W., Farmer J.D., Glassner D.A., Ibsen K.N., Ruth M.F., Schell D.J., Thompson I.B., and Tucker M.P. Bioresour. Technol. 58 (1996) 189
12. Gosselink R.J.A., Vandam J.E.G., and Zomers F.H.A. J. Wood Chem. Technol. 15 (1995) 1
13. Hormeyer H.F., Schwald W., Bonn G., and Bobleter O. Holzforschung 42 (1988) 95
14. Blake J.D., Clarke M.L., and Richards G.N. J. Chromatogr. 398 (1987) 265
15. Xu H., Templeton A.C., and Reed R.A. J. Pharm. Biomed. Anal. 32 (2003) 451
16. Talmadge K.W., Siebert C.J., and Wood R. Am. Lab. 29 (1997) 37
17. Dieter D.S., and Walton H.F. Anal. Chem. 55 (1983) 2109
18. Jupille T., Gray M., Black B., and Gould M. Int. Lab. 11 (1981) 84
19. Wood R., Cummings L., and Jupille T. J. Chromatogr. Sci. 18 (1980) 551
20. Schell D.J., Farmer J., Newman M., and McMillan J.D. Appl. Biochem. Biotechnol. 105 (2003) 69
21. N. Dowe, J.D. McMillan, in: NREL Laboratory Analytical Procedures, US. Department of Energy, Golden, 2001.
22. Cantarella M., Cantarella L., Gallifuoco A., Spera A., and Alfani F. Biotechnol. Prog. 20 (2004) 200
23. Robyt J.F.A. Essentials of Carbohydrate Chemistry (1997), Springer, New York
24. R.A. Mowery, 2009, personal communication.
25. Chen S.F., Mowery R.A., Castleberry V.A., van Walsum G.P., and Chambliss C.K. J. Chromatogr. A 1104 (2006) 54