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3676 For a review on the role of NHC in late transition metal catalysis, see
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2) species, see
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79551703183
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CCDC-800882 (3) and CCDC-800883 (5) contain the supplementary crystallographic data for this contribution. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via.
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CCDC-800882 (3) and CCDC-800883 (5) contain the supplementary crystallographic data for this contribution. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/ data-request/cif.
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-
-
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24
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79551703493
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2) was 0.1261 for 6664 reflections, I > 2σ(I).
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2) was 0.1261 for 6664 reflections, I > 2σ(I).
-
-
-
-
25
-
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33746217434
-
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3869 This is close to the O-O bond distance value of 1.280(3) Å reported for the only other related superoxide structure the authors could locate, that for a Cu complex
-
Würtele, C.; Gaoutchenova, E.; Harms, K.; Holthausen, M. C.; Sundermeyer, J.; Schindler, S. Angew. Chem., Int. Ed. 2006, 45, 3867-3869 This is close to the O-O bond distance value of 1.280(3) Å reported for the only other related superoxide structure the authors could locate, that for a Cu complex
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Würtele, C.1
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26
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76249109920
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Fortman, G. C.; Scott, N. M.; Linden, A.; Stevens, E. D.; Dorta, R.; Nolan, S. P. Chem. Commun. 2010, 46, 1050-1052
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27
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75649103176
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For NHC ligand steric parameters, see
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For NHC ligand steric parameters, see: Clavier, H.; Nolan, S. P. Chem. Commun. 2010, 46, 841-861
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38949179137
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Kelly, R. A., III; Clavier, H.; Guidice, S.; Scott, N. M.; Stevens, E. D.; Bordner, J.; Samardjiev, I.; Hoff, C. D.; Cavallo, L.; Nolan, S. P. Organometallics 2008, 27, 202-210
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33846551900
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Popp, B. V.; Wendlandt, J. E.; Landis, C. R.; Stahl, S. S. Angew. Chem., Int. Ed. 2007, 46, 601-604
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32
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79551697029
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Preliminary stopped-flow studies at -20 ̊C show a biphasic process.
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Preliminary stopped-flow studies at -20 ̊C show a biphasic process.
-
-
-
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34
-
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79551692800
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2) was 0.0375 for 10 468 reflections, I > 2σ(I).
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2) was 0.0375 for 10 468 reflections, I > 2σ(I).
-
-
-
-
35
-
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33745688109
-
-
For a selection of monohydroperoxide structurally characterized complexes, see the following.;,-2907 For Pd-NHC
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For a selection of monohydroperoxide structurally characterized complexes, see the following. Konnick, M. M.; Gandhi, B. A.; Guzei, I. A.; Stahl, S. S. Angew. Chem., Int. Ed. 2006, 45, 2904-2907 For Pd-NHC
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Angew. Chem., Int. Ed.
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, pp. 2904
-
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Konnick, M.M.1
Gandhi, B.A.2
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Stahl, S.S.4
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36
-
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33644638340
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For Pd
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Denney, M. C.; Smythe, N. A.; Cetto, K. L.; Kemp, R. A.; Goldberg, K. I. J. Am. Chem. Soc. 2006, 128, 2508-2509 For Pd
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Denney, M.C.1
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Cetto, K.L.3
Kemp, R.A.4
Goldberg, K.I.5
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37
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64349113645
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For Pt
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Look, J. L.; Wick, D. D.; Mayer, J. M.; Goldberg, K. I. Inorg. Chem. 2009, 48, 1356-1369 For Pt
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Look, J.L.1
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