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For the synthesis of malonate-α,β-unsaturated esters 2a-c we used a modified procedure from
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Crystallographic data for rac -8a and (R,R)- 8d reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC 789982 (rac- 8a) and CCDC 790099 (8d). These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via or on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK [fax.: (internat.) +44-1223/336-033; e-mail: deposit@ ccdc.cam.ac.uk]
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Crystallographic data for rac -8a and (R,R)- 8d reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC 789982 (rac- 8a) and CCDC 790099 (8d). These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via or on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK [fax.: (internat.) +44-1223/336-033; e-mail: deposit@ ccdc.cam.ac.uk].
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