Microwave-assisted preparation of a β-cyclodextrin-based stationary phase for open tubular capillary electrochromatography

Analytical Letters

Volumn 43, Issue 15, 2010, Pages 2372-2380

  Hongjun, E ^a   Su, Ping ^a   Farooq, Muhammad Umar ^a   Yang, Yi ^a  

^a BEIJING UNIVERSITY OF CHEMICAL TECHNOLOGY   (China)

Author keywords

cyclodextrin derivative; Fluorescein isothiocyanate; Microwave assisted; Open tubular capillary electrochromatography

Indexed keywords

EID: 78049326204     PISSN: 00032719     EISSN: 1532236X     Source Type: Journal    
DOI: 10.1080/00032711003725532     Document Type: Article

References (33)

1. Amankwa, L. N., and W. G. Kuhr. 1992. Trypsin-modified fused-silica capillary microreactor for peptide mapping by capillary zone electrophoresis. Anal. Chem. 64: 1610-1613.
2. Armstrong, D. W., Y. Tang, T. Ward, and M. Nichols. 1993. Derivatized cyclodextrins immobilized on fused-Silica capillaries for enantiomeric separations via capillary electrophoresis, gas chromatography, or supercritical fluid chromatography. Anal. Chem. 65: 1114-1117.
3. Caddick, S. 1995. Microwave Assisted Organic Reactions. Tetrahedron 51: 10403-10432.
4. Chen, J., Z. Li, D. Chao, W. Zhang, and C. Wang. 2008. Synthesis of size-tunable metal nanoparticles based on polyacrylonitrile nanofibers enabled by electrospinning and microwave irradiation. Mater. Lett. 62: 692-694.
5. Feibush, B., A. Figueroa, R. Charles, O. P. Feibush, and B. L. Karger. 1986. Chiral separation of heterocyclic drugs by HPLC: Solute-stationary phase base-pair interactions. J. Am. Chem. Soc. 108: 3310-3318.
6. Gong, Y. H., and H. K. Lee. 2002. Enantiomeric separations in capillary electrochromatography with crown ether-capped b-cyclodextrin-bonded silica particles as chiral stationary phase. Helve. Chim. Acta 85: 3283-3293.
7. Gong, Y., and H. K. Lee. 2003. Application of cyclam-capped b-cyclodextrin-bonded silica particles as a chiral stationary phase in capillary electrochromatography for enantiomeric separations. Anal. Chem. 75: 1348-1354.
8. Gubitz, G., and M. G. Schmid. 2008. Chiral separation by capillary electromigration techniques. J. Chromatogr. A 1204: 140-156.
9. Hungerford, G., J. Benesch, J. F. Mano, and R. L. Reis. 2007. Effect of the labelling ratio on the photophysics of fluorescein isothiocyanate (FITC) conjugated to bovine serum albumin. Photochem. Photobiol. Sci. 6: 152-158.
10. Kitagawa, F., K. Inoue, T. Hasegawa, M. Kamiyaa, Y. Okamotoa, M. Kawaseb, and K. Otsuka. 2006. Chiral separation of acidic drug components by open tubular electrochromatography using avidin immobilized capillaries. J. Chromatogr. A 1130: 219-226.
11. Lee, M. J., and C. M. Sun. 2004. Traceless synthesis of hydantoin by focused microwave irradiation. Tetrahedron. Lett. 45: 437-440.
12. Lidstrom, P., J. Tierney, B. Wathey, and J. Westman. 2001. Microwave assisted organic synthesis-a review. Tetrahedron 57: 9225-9283.
13. Lin, B., Z. G. Shi, H. J. Zhang, S. C. Ng, and Y. Feng. 2006. Perphenylcarbamoylated b-cyclodextrin bonded-silica particles as chiral stationary phase for enantioseparation by pressure-assisted capillary electrochromatography. Electrophoresis 27: 3057-3065.
14. Maftouh, M., C. Granier-Loyaux, E. Chavana, J. Marini, A. Pradines, Y. V. Heyden, and C. Picard. 2005. Screening approach for chiral separation of pharmaceuticals part III. supercritical fluid chromatography for analysis and purification in drug discovery. J. Chromatogr. A 1088: 67-81.
15. Maria, C. P., L. C. Antonio, M. M. Luisa, and G. R. Carmen. 2007. Enantioselective separation of azole compounds by EKC. reversal of migration order of enantiomers with CD concentration. Electrophoresis 28: 2667-2674.
16. Nishida, N., H. Yao, and K. Kimura. 2008. Chiral functionalization of optically inactive monolayer-protected silver nanoclusters by chiral ligand-exchange reactions. Langmuir 24: 2759-2766.
17. Nogle, L. M., C. W. Mann, W. L. Watts Jr., and Y. Zhang. 2006. Preparative separation and identification of derivatized b-methylphenylalanine enantiomers by chiral SFC, HPLC and NMR for development of new peptide ligand mimetics in drug discovery. J. Pharm. Biomed. Anal. 40: 901-909.
18. Peng, Z. L., F. Yi, B. Guo, and J. M. Lin. 2007. Temperature effects on the enantioselectivity of basic analytes in capillary EKC using sulfated b-CDs as chiral selectors. Electrophoresis 28: 3753-3758.
19. Phinney, K. W. 2000. Peer reviewed: SFC and drug enantiomers. Anal. Chem. 72: 204-211.
20. Qiao, F. T., and Z. Su. 2002. Analysis of enantiomers of chiral phenethylamine drugs by capillary gas chromatography=mass spectrometry=flame-ionization detection and pre-column chiral derivatization. J. Biochem. Biophy. Meth. 54: 103-113.
21. Sánchez-Hernández, L., A. L. Crego, M. L. Marina, and C. García-Ruiz. 2008. Sensitive chiral analysis by CE: An update. Electrophoresis 29: 237-251.
22. Sadeghi, A. A., and P. Shawrang. 2008. Effects of microwave irradiation on luminal dry matter, protein and starch degradation characteristics of barley grain. Anim. Feed. Sci. Tech. 141: 184-194.
23. Schurig, V., and D. Wistuba. 1999. Recent innovations in enantiomer separation by electro chromatography utilizing modified cyclodextrins as stationary phase. Electrophoresis 20: 2313-2328.
24. Son, Y. J., J. S. Jang, Y. W. Cho, H. Chung, R. W. Park, I. C. Kwon, I. S. Kim, et al. 2003. Biodistribution and anti-tumor efficacy of doxorubicin loaded glycol-chitosan nanoaggregates by EPR effect. J. Control. Rel. 91: 135-145.
25. Vargas-Diaz, M. E., L. Chacon-Garcia, P. Velazquez, J. Tamari, P. Joseph-Nathanb, and L. G. Zepeda. 2003. Enantioselective synthesis of 1-alkyl-substituted 1-phenyl-1, 2-ethanediols using a myrtenal-derived chiral auxiliary. Tetrahedron 14: 3225-3232.
26. Wang, Z. Z., J. Ouyang, and W. R. G. Baeyens. 2008. Recent developments of enantioseparation techniques for adrenergic drugs using liquid chromatography and capillary electrophoresis: A review. J. Chromatogr. B 862: 1-14.
27. Wang, Y., Z. Zeng, N. Guan, and J. Cheng. 2001. Sol-gel technique for the preparation of b-cyclodextrin derivative stationary phase in open-tubular capillary electrochromatography. Electrophoresis 22: 2167-2172.
28. Wistuba, D., and V. Schurig. 1999. Enantiomer separation by pressure-supported electrochromatography using capillaries packed with chirasil-Dex polymer-coated silica. Electrophoresis 20: 2779-2785.
29. Wistuba, D., and V. Schurig. 2006. Comparison of monolithic approaches for enantioselective capillary electrochromatography involving cyclodextrins. J. Sep. Sci. 29: 1344-1352.
30. Xu, L., and Y. Sun. 2007. Fabrication and characterization of open-tubular CEC modified with tentacle-type metal-chelating polymer chains. Electrophoresis 28: 1658-1667.
31. Zhang, X. X., F. Hong, W. B. Chang, Y. X. Ci, and Y. H. Ye. 1999. Enantiomeric separation of promethazine and D, L-a-amino-b-[4-(1,2-dihydro-2-oxo-quinoline)] propionic acid drugs by capillary zone electrophoresis using albumin as chiral selectors. Anal. Chim. Acta 392: 175-181.
32. Zhang, Y. P., X. W. Ye, M. K. Tian, L. B. Qu, S. H. Choi, A. I. Gopalan, and K. P. Lee. 2008. Novel method to prepare polystyrene-based monolithic columns for chromatographic and electrophoretic separations by microwave irradiation. J. Chromatogr. A 1188: 43-49.
33. Zhang, Z. S., and Y. Yang. 2006. Preparation and evaluation of open-tubular capillary electrochromatography column with the poly (amidoamine) (PAMAM) dendrimers as bonded stationary phase. Chem. J. Chin. U. 27: 47-51.