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Volumn 51, Issue 33, 2010, Pages 4466-4469

Synthesis of tetralin and chromane derivatives via In-catalyzed intramolecular hydroarylation

Author keywords

[No Author keywords available]

Indexed keywords

CHROMAN DERIVATIVE; INDIUM; TETRALIN DERIVATIVE;

EID: 77955421936     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2010.06.091     Document Type: Article
Times cited : (30)

References (81)
  • 31
  • 76
    • 77955427317 scopus 로고    scopus 로고
    • note
    • 2 until TLC indicated the complete consumption of the starting material. The reaction mixture was cooled to rt and the mixture was filtered through a plug of silica gel. The evaporation of the solvent gave the desired product 1-methyl-tetralin A in >97% yield. The product was identified by NMR and MS analysis and the data are consistent with the reported values.
  • 77
    • 53949088904 scopus 로고    scopus 로고
    • For some recent reviews on C-H activation, please see: F. Kakiuchi, and T. Kochi Synthesis 2008 3013
    • (2008) Synthesis , pp. 3013
    • Kakiuchi, F.1    Kochi, T.2
  • 81
    • 77955431335 scopus 로고    scopus 로고
    • note
    • The pH value of the reaction system, at the beginning of the reaction, was measured to be around 6. However, it changed to 2 after one hour and remained around 2 afterward.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.