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CCDC 771775 (5a), 771776 (5b), 771777 (9), and 771778 (10) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via
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CCDC 771775 (5a), 771776 (5b), 771777 (9), and 771778 (10) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data-request/cif.
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49
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We examined the thermal reaction of 5b in xylene at reflux, but the reaction did not occur. This failure is probably a result of steric hindrance from the tBu group ortho to the Pt-O group in the formation of the intermediate corresponding to 13
-
We examined the thermal reaction of 5b in xylene at reflux, but the reaction did not occur. This failure is probably a result of steric hindrance from the tBu group ortho to the Pt-O group in the formation of the intermediate corresponding to 13.
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