Multi-residue method for the determination of organochlorine pesticides in fish feed based on a cleanup approach followed by gas chromatography-triple quadrupole tandem mass spectrometry

Journal of Chromatography A

Volumn 1217, Issue 30, 2010, Pages 4996-5003

  Nardelli, Valeria ^a   dell'Oro, Daniela ^a   Palermo, Carmen ^b   Centonze, Diego ^b  

^a ISTITUTO ZOOPROFILATTICO SPERIMENTALE DELLA PUGLIA E DELLA BASILICATA   (Italy)

^b UNIVERSITY OF FOGGIA   (Italy)

Author keywords

Cleanup; Fish feed; GC MS MS; Multi residue method; Organochlorine pesticides; SPE

Indexed keywords

CALIBRATION CURVES; CLEANUP APPROACH; DIATOMACEOUS EARTH; FISH FEED; GC-MS/MS; INTERFERING SUBSTANCES; LIMITS OF DETECTION; LINEAR RANGE; LIQUID-LIQUID EXTRACTION; MATRIX EFFECTS; ORGANOCHLORINE PESTICIDES; PERFORMANCE CHARACTERISTICS; RELATIVE STANDARD DEVIATIONS; SOLID-PHASE EXTRACTION; TRIPLE QUADRUPOLE; TRIPLE QUADRUPOLE TANDEM MASS SPECTROMETRY;

AGRICULTURAL CHEMICALS; FISH; GAS CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETRY; PESTICIDES; PROJECTILES; SILICA; SILICA GEL; SOLVENT EXTRACTION;

CHEMICAL CONTAMINATION;

ACETONITRILE; HEXANE; ORGANOCHLORINE PESTICIDE; SILICA GEL; CHLORINATED HYDROCARBON; PESTICIDE RESIDUE;

ACCURACY; ARTICLE; CALIBRATION; CONTROLLED STUDY; FISH; FOOD ANALYSIS; FOOD CONTAMINATION; GAS CHROMATOGRAPHY; LIQUID LIQUID EXTRACTION; NONHUMAN; PRIORITY JOURNAL; PROCESS DEVELOPMENT; PROCESS OPTIMIZATION; PRODUCT RECOVERY; QUADRUPOLE MASS SPECTROMETRY; QUANTITATIVE ANALYSIS; REPRODUCIBILITY; RESIDUE ANALYSIS; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; ANIMAL; EVALUATION; MASS FRAGMENTOGRAPHY; METHODOLOGY; SEA FOOD; STATISTICAL PARAMETERS;

ANIMALS; FISHES; FOOD CONTAMINATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HYDROCARBONS, CHLORINATED; LIMIT OF DETECTION; PESTICIDE RESIDUES; SEAFOOD; TANDEM MASS SPECTROMETRY;

EID: 77954175017     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.05.052     Document Type: Article

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