Development and validation of a liquid chromatography-tandem mass spectrometry assay for the simultaneous quantitation of microcystin-RR and its metabolites in fish liver

Journal of Chromatography A

Volumn 1217, Issue 9, 2010, Pages 1455-1462

  Wu, Laiyan ^a   Xie, Ping ^a   Chen, Jun ^a   Zhang, Dawen ^a   Liang, Gaodao ^a  

^a INSTITUTE OF HYDROBIOLOGY   (China)

Author keywords

LC MS MS; Method validation; Microcystin; SPE

Indexed keywords

AMMONIA SOLUTION; ANALYTES; BIGHEAD CARP; CATION EXCHANGES; DRY WEIGHT; ELECTROSPRAY IONIZATION ION TRAP MASS SPECTROMETRY; LC-MS/MS; LIMITS OF QUANTIFICATION; LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY ASSAYS; METHOD DETECTION LIMITS; METHOD VALIDATIONS; MICROCYSTINS; MIXED MODE; NOVEL METHODS;

CHROMATOGRAPHIC ANALYSIS; DIELECTRIC WAVEGUIDES; ELECTROSPRAY IONIZATION; ION EXCHANGE; LIQUID CHROMATOGRAPHY; LIQUIDS; LIVER; MASS SPECTROMETERS; MASS SPECTROMETRY; MEATS; METABOLISM; METABOLITES; METHANOL; SOLAR RADIATION;

SEMICONDUCTOR COUNTERS;

ACETIC ACID; AMMONIA; EDETIC ACID; METHANOL; MICROCYSTIN RR; MICROCYSTIN RR CYSTEINE; MICROCYSTIN RR GLUTATHIONE; UNCLASSIFIED DRUG;

ANIMAL TISSUE; ARTICLE; CARP; CONTROLLED STUDY; DRY WEIGHT; ELECTROSPRAY MASS SPECTROMETRY; ENVIRONMENTAL EXPOSURE; FOOD ANALYSIS; FOOD SAFETY; ION TRAP MASS SPECTROMETRY; LIQUID CHROMATOGRAPHY; LIVER PARENCHYMA; NONHUMAN; PH; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; SENSITIVITY AND SPECIFICITY; SOLVENT EXTRACTION; TANDEM MASS SPECTROMETRY; VALIDATION PROCESS;

ANIMALS; CARPS; CHROMATOGRAPHY, LIQUID; ENVIRONMENTAL MONITORING; LIMIT OF DETECTION; LIVER; METHANOL; MICROCYSTINS; SOLID PHASE EXTRACTION; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TANDEM MASS SPECTROMETRY; TIME FACTORS;

HYPOPHTHALMICHTHYS;

EID: 75349102818     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2009.12.068     Document Type: Article

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