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73649128354
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Crystal data for l-E: C50H24B2F 30N, Mr= 1230.32, triclinic, Pl, a, 11.7619(4) Å, b, 11.9617(4) Å, c, 20.1408(7) Å, α, 84.658(3)°, β, 75.635(3)°, γ, 60.642(4)°, V, 2391.16(17) Å3, Z, 2, Dc, 1.709 g cm -3, μ, 0.181 mm-1, γ, 0.71073 Å, T= 183(2) K, 30688 reflections collected, 9745 independent (Rint, 0.0567) and 5597 observed reflections (I > 2σI, 749 refined parameters, R1, 0.0410, wR2, 0.08919. CCDC 748013
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-1, γ = 0.71073 Å, T= 183(2) K, 30688 reflections collected, 9745 independent (Rint = 0.0567) and 5597 observed reflections (I > 2σ(I)), 749 refined parameters, R1 = 0.0410, wR2 = 0.08919. CCDC 748013.
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34
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73649088678
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Crystal data for 2-E: C39H37BF 15P, Mr, 832.47, monoclinic, P21/c, a, 12.3469(2) Å,b, 18.0538(2) Å, c, 17.8463(2) Å, β, 104.935(2)°, V, 3843.71(9) Å3, Z, 4, Dc, 1.439gcm-3, λ, 0.173 mm -1, λ, 0.710 73 Å, T= 183(2) K, 33 277 reflections collected, 7864 independent (Rint, 0.026) and 5618 observed reflections (I > 2σI, 523 refined parameters, R1, 0.050, wR2, 0.134. CCDC 748014
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-1, λ = 0.710 73 Å, T= 183(2) K, 33 277 reflections collected, 7864 independent (Rint = 0.026) and 5618 observed reflections (I > 2σ(I)), 523 refined parameters, R1 = 0.050, wR2 = 0.134. CCDC 748014.
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0034740448
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Graton, J.; Berthelot, M.; Laurence, C. J. Chem. Soc., Perkin Trans. 2001, 2130.
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Graton, J.1
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73649113852
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Crystal data for 5: C35H55BF15N, M r, 755.37, triclinic, P1, a, 10.2056(11)Å, b, 12.2576(8)A,c, 14.6323(8) Å, α, 70.676(3)°, β, 87.904(3)°, γ, 68.808(4)°, V, 1603.3(2) Å3, Z, 2, Dc, 1.565 g cm-3, μ, 0.152 mm-1, λ, 0.71073Å, T= 183(2) K, 20 184 reflections collected, 7943 independent (Rint, 0.0320) and 5663 observed reflections (I > 2σI, 481 refined parameters, R1, 0.0388, wR2, 0.0904. CCDC 748015
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int = 0.0320) and 5663 observed reflections (I > 2σ(I)), 481 refined parameters, R1 = 0.0388, wR2 = 0.0904. CCDC 748015.
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39
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73649096929
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int = 0.0241) and 7111 observed reflections (I > 2σ(I)), 473 refined parameters, R1 = 0.0401, wR2 = 0.1114. CCDC 748016.
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int = 0.0241) and 7111 observed reflections (I > 2σ(I)), 473 refined parameters, R1 = 0.0401, wR2 = 0.1114. CCDC 748016.
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66149139746
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