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Angewandte Chemie - International Edition
Volumn 38, Issue 22, 1999, Pages 3362-3365
Treatment of naphthols with B(C6F5)3: Formation and characterization of the Lewis acid adducts of their keto isomers
Author keywords

Boron; Hydrozirconations; Lewis acids naphthols; Tautomerism
Indexed keywords

1 NAPHTHOL; BORANE DERIVATIVE; BORON;
EID: 0344286527     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1521-3773(19991115)38:22<3362::AID-ANIE3362>3.0.CO;2-N     Document Type: Article
Times cited : (47)
References (55)
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    • (Engl. Transl. 1998, 34, 595), and references therein
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    • 3; hydrogen atoms were calculated and refined as riding atoms. The structure contains two toluene molecules in the asymmetric unit. The data set was collected with a Nonius KappaCCD diffractometer on a rotating anode generator (FR 591). Programs used: data acquisition: COLLECT (Nonius B. V., 1998), data reduction: Denzo-SMN (Z. Otwinowski, W. Minor, Methods Enzymol. 1997, 276, 307-326), absorption correction: SORTAV (R. H. Blessing, Acta Crystallogr. Sect. A 1995, 51, 33-37; R. H. Blessing, J. Appl. Cryst. 1997, 30, 421-426), structure solution: SHELXS-97 (G. M. Sheldrick, Acta Crystallogr. Sect. A 1990, 46, 467-473), structure refinement: SHELXL-97, graphics: SCHAKAL-92.
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    • 3; hydrogen atoms were calculated and refined as riding atoms. The structure contains two toluene molecules in the asymmetric unit. The data set was collected with a Nonius KappaCCD diffractometer on a rotating anode generator (FR 591). Programs used: data acquisition: COLLECT (Nonius B. V., 1998), data reduction: Denzo-SMN (Z. Otwinowski, W. Minor, Methods Enzymol. 1997, 276, 307-326), absorption correction: SORTAV (R. H. Blessing, Acta Crystallogr. Sect. A 1995, 51, 33-37; R. H. Blessing, J. Appl. Cryst. 1997, 30, 421-426), structure solution: SHELXS-97 (G. M. Sheldrick, Acta Crystallogr. Sect. A 1990, 46, 467-473), structure refinement: SHELXL-97, graphics: SCHAKAL-92.
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    • 3; hydrogen atoms were calculated and refined as riding atoms. The structure contains two toluene molecules in the asymmetric unit. The data set was collected with a Nonius KappaCCD diffractometer on a rotating anode generator (FR 591). Programs used: data acquisition: COLLECT (Nonius B. V., 1998), data reduction: Denzo-SMN (Z. Otwinowski, W. Minor, Methods Enzymol. 1997, 276, 307-326), absorption correction: SORTAV (R. H. Blessing, Acta Crystallogr. Sect. A 1995, 51, 33-37; R. H. Blessing, J. Appl. Cryst. 1997, 30, 421-426), structure solution: SHELXS-97 (G. M. Sheldrick, Acta Crystallogr. Sect. A 1990, 46, 467-473), structure refinement: SHELXL-97, graphics: SCHAKAL-92.
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    • 3; hydrogen atoms were calculated and refined as riding atoms. The structure contains two toluene molecules in the asymmetric unit. The data set was collected with a Nonius KappaCCD diffractometer on a rotating anode generator (FR 591). Programs used: data acquisition: COLLECT (Nonius B. V., 1998), data reduction: Denzo-SMN (Z. Otwinowski, W. Minor, Methods Enzymol. 1997, 276, 307-326), absorption correction: SORTAV (R. H. Blessing, Acta Crystallogr. Sect. A 1995, 51, 33-37; R. H. Blessing, J. Appl. Cryst. 1997, 30, 421-426), structure solution: SHELXS-97 (G. M. Sheldrick, Acta Crystallogr. Sect. A 1990, 46, 467-473), structure refinement: SHELXL-97, graphics: SCHAKAL-92.
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    • note
    • 3: hydrogen atoms were calculated and refined as riding atoms. The data set was collected with a Nonius KappaCCD diffractometer on a rotating anode generator (FR 591). d) Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication nos. CCDC-120955 (3), -120956 (5), and -120957 (9). Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: (+ 44) 1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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