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note
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Representative procedure for the enantioselective aldol reaction with catalyst 10: A mixture of catalyst 10 (31 mg, 0.13 mmol), cyclohexanone (646 mg, 6.6 mmol), and TFA (7.5 mg, 0.066 mmol) contained in 1.0 mL of DMF (1.0 mL) was stirred at room temperature for 45 min. Subsequently, the temperature was brought down to 3 °C and the aldehyde (100 mg, 0.66 mmol) was introduced. The reaction mixture was stirred at 3 °C until the reaction was judged to be complete, based on TLC analysis. The reaction mixture was directly passed through a short silica gel column to isolate the pure aldol product.
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