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Crystal data for compound 4:C19H3Cl 9N2S2, yellow, M, 642.40, triclinic, space group P1̄, a, 8.3193(7) Å, b, 11.2070(8) Å, c, 12.0009(9) Å, V, 1086.75 (14) Å3, Z, 2, T, 173(2) K, Dc, 1.963 g cm -3, μ(MoKa, 1.367 mm-1, 9534 reflections collected, 4198 are independent (Rint, 0.1071, The final agreement factors are R1, 0.0381 (I > 2σI, with 1891 data and wR2, 0.0607 for 4198 data based on 289 parameters
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