Colloidal chemical synthesis and formation kinetics of uniformly sized nanocrystals of metals, oxides, and chalcogenides

Accounts of Chemical Research

Volumn 41, Issue 12, 2008, Pages 1696-1709

  Soon, Gu Kwon ^a   Hyeon, Taeghwan ^a  

^a Seoul National University   (South Korea)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 58149095488     PISSN: 00014842     EISSN: None     Source Type: Journal    
DOI: 10.1021/ar8000537     Document Type: Article

References (39)

1. Park, J.; Joo, J.; Kwon, S. G.; Jang, Y.; Hyeon, T. Synthesis of Monodisperse Spherical Nanocrystals. Angew. Chem., Int. Ed. 2007, 46, 4630-4660.
2. El-Sayed, M. A. Small Is Different: Shape-, Size-, and Composition-Dependent Properties of Some Colloidal Semiconductor Nanocrystals. Acc. Chem. Res. 2004, 37, 326-333.
3. Klimov, V. I., Ed. Semiconductor and Metal Nanocrystals; Marcel Dekker, Inc.: New York, 2004.
4. Murray, C. B.; Norris, D. J.; Bawendi, M. G. Synthesis and Characterization of Nearly Monodisperse CdE(E)S, Se, Te) Semiconductor Nanocrystallites. J. Am. Chem. Soc. 1993, 115, 8706-8715.
5. Peng, X.; Wickham, J.; Alivisatos, A. P. Kinetics of II-VI and III-V Colloidal Semiconductor Nanocrystal Growth: "Focusing" of Size Distributions. J. Am. Chem. Soc. 1998, 120, 5343-5344.
6. Donegá, C. d. M.; Liljeroth, P.; Vanmaekelbergh, D. Physicochemical Evaluation of the Hot-Injection Method, a Synthesis Route for Monodisperse Nanocrystals. Small 2005, 1, 1152-1162.
7. Sun, S.; Murray, C. B.; Weller, D.; Folks, L.; Moser, A. Monodisperse FePt Nanoparticles and Ferromagnetic FePt Nanocrystal Superlattices. Science 2000, 287, 1989-1992.
8. 1 Contrast Agent for Magnetic Resonance Imaging Using MnO Nanoparticles. Angew. Chem., Int. Ed. 2007, 46, 5397-5401.
9. Park, S. J.; Kim, S.; Lee, S.; Khim, Z. G.; Char, K.; Hyeon, T. Synthesis and Magnetic Studies of Uniform Iron Nanorods and Nanospheres. J. Am. Chem. Soc. 2000, 122, 8581-8582.
10. Hyeon, T.; Lee, S. S.; Park, J.; Chung, Y.; Na, H. B. Synthesis of Highly Crystalline and Monodisperse Maghemite Nanocrystallites without a Size-Selection Process. J. Am. Chem. Soc. 2001, 123, 12798-12801.
11. Park, J.; Lee, E.; Hwang, N. M.; Kang, M.; Kim, S. C.; Hwang, Y.; Park, J. G.; Noh, H. J.; Kim, J. Y.; Park, J. H.; Hyeon, T. One-Nanometer-Scale Size-Controlled Synthesis of Monodisperse Magnetic Iron Oxide Nanoparticles. Angew. Chem., Int. Ed. 2005, 44, 2872-2877.
12. x Alloy Particles. J. Colloid Interface Sci. 1988, 121, 558-563.
13. Casula, M. F.; Jun, Y.-w.; Zaziski, D. J.; Chan, E. M.; Corrias, A.; Alivisatos, A. P. The Concept of Delayed Nucleation in Nanocrystal Growth Demonstrated for the Case of Iron Oxide Nanodisks. J. Am. Chem. Soc. 2006, 128, 1675-1682.
14. Hyeon, T.; Chung, Y.; Park, J.; Lee, S. S.; Kim, Y. W.; Park, B. H. Synthesis of Highly Crystalline and Monodisperse Cobalt Ferrite Nanocrystals. J. Phys. Chem. B 2002, 106, 6831-6833.
15. Kang, E.; Park, J.; Hwang, Y.; Kang, M.; Park, J. G.; Hyeon, T. Direct Synthesis of Highly Crystalline and Monodisperse Manganese Ferrite Nanocrystals. J. Phys. Chem. B 2004, 108, 13932-13935.
16. Park, J.; An, K.; Hwang, Y.; Park, J. G.; Noh, H. J.; Kim, J. Y.; Park, J. H.; Hwang, N. M.; Hyeon, T. Ultra-Large-Scale Syntheses of Monodisperse Nanocrystals. Nat. Mater. 2004, 3, 891-895.
17. Choi, S. H.; Kim, E. G.; Park, J.; An, K.; Lee, N.; Kim, S. C.; Hyeon, T. Large-Scale Synthesis of Hexagonal Pyramid-Shaped ZnO Nanocrystals from Thermolysis of Zn-Oleate Complex. J. Phys. Chem. B 2005, 109, 14792-14794.
18. An, K.; Lee, N.; Park, J.; Kim, S. C.; Hwang, Y.; Park, J. G.; Kim, J. Y.; Park, J. H.; Han, M. J.; Yu, J.; Hyeon, T. Synthesis, Characterization, and Self-Assembly of Pencil-Shaped CoO Nanorods. J. Am. Chem. Soc. 2006, 128, 9753-9760.
19. Kim, D.; Park, J.; An, K.; Yang, N. K.; Park, J. G.; Hyeon, T. Synthesis of Hollow Iron Nanoframes. J. Am. Chem. Soc. 2007, 129, 5812-5813.
20. Kwon, S. G.; Piao, Y.; Park, J.; Angappane, S.; Jo, Y.; Hwang, N. M.; Park, J. G.; Hyeon, T. Kinetics of Monodisperse Iron Oxide Nanocrystal Formation by Heating-Up Process. J. Am. Chem. Soc. 2007, 129, 12571-12584.
21. Talapin, D. V.; Rogach, A. L.; Haase, M.; Weller, H. Evolution of an Ensemble of Nanoparticles in a Colloidal Solution: Theoretical Study. J. Phys. Chem. B 2001, 105, 12278-12285.
22. Sugimoto, T. Preparation of Monodisperse Colloidal Particles. Adv. Colloid Interfac. Sci. 1987, 28, 65-108.
23. Brinker, C. J.; Scherer, G. W. Sol-Gel Science; Academic Press: Boston, 1990.
24. Vioux, A. Nonhydrolytic Sol-Gel Routes to Oxides. Chem. Mater. 1997, 9, 2292-2299.
25. Niederberger, M. Nonaqueous Sol-Gel Routes to Metal Oxide Nanoparticles. Acc. Chem. Res. 2007, 40, 793-800.
26. Joo, J.; Yu, T.; Kim, Y. W.; Park, H. M.; Wu, F.; Zhang, J. Z.; Hyeon, T. Multigram Scale Synthesis and Characterization of Monodisperse Tetragonal Zirconia Nanocrystals. J. Am. Chem. Soc. 2003, 125, 6553-6557.
27. 2 Nanocrystals by Nonhydrolytic Solution-Based Reactions. J. Am. Chem. Soc. 1999, 121, 1613-1614.
28. Joo, J.; Kwon, S. G.; Yu, J. H.; Hyeon, T. Synthesis of ZnO Nanocrystals with Cone, Hexagonal Cone, and Rod Shapes via Non-Hydrolytic Ester Elimination Sol-Gel Reactions. Adv. Mater. 2005, 17, 1873-1877.
29. 2 Nanorods via Nonhydrolytic Sol-Gel Ester Elimination Reaction and Their Application to Photocatalytic Inactivation of E. coli. J. Phys. Chem. B 2005, 109, 15297-15302.
30. Kim, S. W.; Park, J.; Jang, Y.; Chung, Y.; Hwang, S.; Hyeon, T.; Kim, Y. W. Synthesis of Monodisperse Palladium Nanoparticles. Nano Lett. 2003, 3, 1289-1291.
31. Blanchard, G. J.; Newman, J. D. S. Formation of Gold Nanoparticles Using Amine Reducing Agents. Langmuir 2006, 22, 5882-5887.
32. Esumi, K.; Tano, T.; Meguro, K. Preparation of Organopalladium Particles from Thermal Decomposition of Its Organic Complex in Organic Solvents. Langmuir 1989, 5, 268-270.
33. Son, S. U.; Jang, Y.; Park, J.; Na, H. B.; Park, H. M.; Yun, H. J.; Lee, J.; Hyeon, T. Designed Synthesis of Atom-Economical Pd/Ni Bimetallic Nanoparticle-Based Catalysts for Sonogashira Coupling Reactions. J. Am. Chem. Soc. 2004, 126, 5026-5027.
34. 2O Coated Cu Nanoparticles and Their Successful Applications to Ullmann-Type Amination Coupling Reactions of Aryl Chlorides. Chem. Commun. 2004, 778, 779.
35. Park, J.; Kang, E.; Son, S. U.; Park, H. M.; Lee, M. K.; Kim, J.; Kim, K. W.; Noh, H. J.; Park, J. H.; Bae, C. J.; Park, J. G.; Hyeon, T. Monodisperse Nanoparticles of Ni and NiO: Synthesis, Characterization, Self-Assembled Superlattices, and Catalytic Applications in the Suzuki Coupling Reaction. Adv. Mater. 2005, 17, 429-434.
36. Joo, J.; Na, H. B.; Yu, T.; Yu, J. H.; Kim, Y. W.; Wu, F.; Zhang, J. Z.; Hyeon, T. Generalized and Facile Synthesis of Semiconducting Metal Sulfide Nanocrystals. J. Am. Chem. Soc. 2003, 125, 11100-11105.
37. Davis, R. E.; Nakshbendi, H. F. Sulfur in Amine Solvents. J. Am. Chem. Soc. 1962, 84, 2085-2090.
38. Sonoda, N.; Yasuhara, T.; Kondo, K.; Ikeda, T.; Tsutsumi, S. A New Synthesis of Ureas. The Reaction of Ammonia or Aliphatic Amines with Carbon Monoxide in the Presence of Selenium. J. Am. Chem. Soc. 1971, 93, 6344.
39. Joo, J.; Son, J. S.; Kwon, S. G.; Yu, J. H.; Hyeon, T. Low-Temperature Solution-Phase Synthesis of Quantum Well Structured CdSe Nanoribbons. J. Am. Chem. Soc. 2006, 128, 5632-5633.