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The enantioselectivity was determined by Chiral-HPLC (CHIRALPAK OJ-H, 254 nm) by deprotecting the acetate group and converting the free alcohol group to its benzoate ester.
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The enantioselectivity was determined by Chiral-HPLC (CHIRALPAK OJ-H, 254 nm) by deprotecting the acetate group and converting the free alcohol group to its benzoate ester.
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The enantioselectivity of this step was determined by measuring the specific rotation value of 1,3-butanediol (obtained from 10 after successive deprotection of acetate and PMB group) and comparing with that of authentic sample.
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The enantioselectivity of this step was determined by measuring the specific rotation value of 1,3-butanediol (obtained from 10 after successive deprotection of acetate and PMB group) and comparing with that of authentic sample.
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23
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