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Tetrahedron Letters

Volumn 51, Issue 1, 2010, Pages 43-45

Iron-catalyzed conversion of unactivated aryl halides to phenols in water

(6) Ren, Yunlai a Cheng, Lin a Tian, Xinzhe a Zhao, Shuang a Wang, Jianji a Hou, Chaodong a

a HENAN UNIVERSITY OF SCIENCE AND TECHNOLOGY (China)

Author keywords

Aryl halide; Iron; Phenol; Water

Indexed keywords

BROMIDE; BROMOBENZENE; FERROUS CHLORIDE; HALIDE; IRON DERIVATIVE; PHENANTHROLINE; PHENOL DERIVATIVE; POLYCYCLIC AROMATIC HYDROCARBON DERIVATIVE; SOLVENT; WATER;

ARTICLE; ARYLATION; CATALYST; CROSS COUPLING REACTION; SUBSTITUTION REACTION; SYNTHESIS;

EID: 70649095246 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/j.tetlet.2009.10.036 Document Type: Article

Times cited : (31)

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- General experimental procedure for Iron-catalyzed conversion of aryl halides to phenols: FeCl3 (0.2 mmol, purchased from Aladdin Reagent Co, purity >98, Cu <10 ppm, ligand (1 mmol) and TBAF (1 mmol) were added to a 10 mL stainless steel autoclave containing H2O (3 mL, After the mixture was stirred at room temperature for 5 min to give a homogeneous solution, K3PO4·3H2O (2 mmol) and aryl halide (1 mmol) were added. Subsequently, the sealed autoclave was placed in a 180 °C oil bath stirred for 20 h the pressure that created on the sealed autoclave was about 0.7 MPa, The desired product was extracted with 3 × 5 mL of diethyl ether. Evaporation of the solvent was followed by the GC analysis of the product. The product was purified by column chromatography. All the products are known compounds and were identified by comparison of their 1H NMR and 13C NMR data with the literature data
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