Accurate quantitative isotopic 13C NMR spectroscopy for the determination of the intramolecular distribution of 13C in glucose at natural abundance

Analytical Chemistry

Volumn 81, Issue 21, 2009, Pages 8978-8985

  Gilbert, Alexis ^a   Silvestre, Virginie ^a   Robins, Richard J ^a   Remaud, Gérald S ^a  

^a UNIVERSITÉ DE NANTES   (France)

Author keywords

[No Author keywords available]

Indexed keywords

ANOMERIZATION; CARBON ATOMS; INTRAMOLECULAR DISTRIBUTION; ISOPROPYLIDENE; ISOTOPE DISTRIBUTIONS; ISOTOPE RATIO; METABOLIC PATHWAYS; MOLECULAR PROBES; NATURAL ABUNDANCE; NMR SIGNALS; NMR SPECTROMETRY; NMR SPECTROSCOPY; SITE-SPECIFIC; STANDARD DEVIATION; THREE-STEP SYNTHESIS;

FRUCTOSE; ISOTOPES; METABOLISM; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SUGAR (SUCROSE);

GLUCOSE;

3,5,6 TRIACETYL 1,2 O ISOPROPYLIDENE ALPHA DEXTRO GLUCOFURANOSE; CARBON 13; FRUCTOSE; GLUCOSE DERIVATIVE; SUCROSE; UNCLASSIFIED DRUG;

ACCURACY; ARTICLE; BIOSYNTHESIS; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL STRUCTURE; ENZYME METABOLISM; METABOLITE; MOLECULAR PROBE; QUANTITATIVE ANALYSIS; RADIOISOTOPE DISTRIBUTION;

CARBON ISOTOPES; GLUCOSE; MAGNETIC RESONANCE SPECTROSCOPY;

EID: 70350639282     PISSN: 00032700     EISSN: None     Source Type: Journal    
DOI: 10.1021/ac901441g     Document Type: Article

References (31)

1. O'Leary, M. H.; Madhavan, S.; Paneth, P. Plant, Cell Environ. 1992, 15, 1099-1104.
2. Brugnoli, E.; Farquhar, G. D. In Photosynthesis: Physiology and Metabolism; Kluwer Academic Publishers: Alphen aan den Rijn, The Netherlands, 2000, pp 399-434.
3. Rossmann, A.; Butzenlechner, M.; Schmidt, H. L. Plant Physiol. 1991, 96, 609-614.
4. Caytan, E.; Botosoa, E. P.; Silvestre, V.; Robins, R. J.; Akoka, S.; Remaud, G. S. Anal. Chem. 2007, 79, 8266-8269.
5. Mauve, C.; Bleton, J.; Bathellier, C.; Lelarge-Trouverie, C.; Guérard, F.; Ghashghaie, J.; Tchapla, A.; Tcherkez, G. Rapid Commun. Mass Spectrom. 2009, 23, 2499-2506.
6. Caytan, E.; Cherghaoui, Y.; Barril, C.; Jouitteau, C.; Rabiller, C.; Remaud, G. Tetrahedron: Asymmetry 2006, 17, 1622-1624.
7. Tenailleau, E.; Akoka, S. J. Magn. Reson. 2007, 185, 50-58.
8. Tenailleau, E.; Remaud, G.; Akoka, S. Instrum. Sci. Technol. 2005, 33, 391-399.
9. Caytan, E.; Remaud, G. S.; Tenailleau, E.; Akoka, S. Talanta 2007, 71, 1016-1021.
10. Schleucher, J.; Vanderveer, P.; Markley, J. L.; Sharkey, T. D. Plant, Cell Environ. 1999, 22, 525-533.
11. Zhang, B. L.; Billault, I.; Lo, X. B.; Mabon, F.; Remaud, G.; Martin, M. L. J. Agric. Food Chem. 2002, 50, 1574-1580.
12. Silvestre, V.; Mboula, V. M.; Jouitteau, C.; Akoka, S.; Robins, R. J.; Remaud, G. S. J. Chromatogr., A 2009, 1216, 7043-7048.
13. Tenailleau, E.; Lancelin, P.; Robins, R. J.; Akoka, S. Anal. Chem. 2004, 76, 3818-3825.
14. Hyvönen, L.; Varo, P.; Koivistoinen, P. J. Food Sci. 1977, 42, 657-659.
15. Yamabe, S.; Ishikawa, T. J. Org. Chem. 1999, 64, 4519-4524.
16. Botosoa, E. P.; Silvestre, V.; Robins, R. J.; Rojas, J. M. M.; Guillou, C.; Remaud, G. S. J. Chromatogr., A, in press. DOI: 10.1016/j.chroma.2009.08. 066.
17. Luboradzki, R.; Pakulski, Z.; Sartowska, B. Tetrahedron 2005, 61, 10122-10128.
18. Gronwald, O.; Sakurai, K.; Luboradzki, R.; Kimura, T.; Shinkai, S. Carbohydr. Res. 2001, 331, 307-318.
19. Tritt-Goc, J.; Bielejewski, M.; Luboradzki, R.; Lapinski, A. Langmuir 2008, 24, 534-540.
20. Reuben, J. J. Am. Chem. Soc. 1984, 106, 6180-6186.
21. Reuben, J. J. Am. Chem. Soc. 1985, 107, 1747-1755.
22. Doner, L. W.; Ajie, H. O.; Sternberg, L. d. S. L.; Milburn, J. M.; DeNiro, M. J.; Hicks, K. B. J. Agric. Food Chem. 1987, 35, 610-612.
23. Gonzalez, J.; Remaud, G.; Jamin, E.; Naulet, N.; Martin, G. G. J. Agric. Food Chem. 1999, 47, 2316-2321.
24. Hayashi, F. J. Biochem. 1932, 16, 1-16.
25. Whistler, R. L.; Durso, D. F. J. Am. Chem. Soc. 1950, 72, 677-679.
26. Menditto, A.; Patriarca, M.; Magnusson, B. Accredit. Qual. Assur. 2007, 12, 45-47.
27. Zhang, B.-L.; Trierweiler, M.; Jouitteau, C.; Martin, G. J. Anal. Chem. 1999, 71, 2301-2306.
28. Danilova, V. A.; Krivdin, L. B. Russ. J. Org. Chem. 2003, 39, 1764-1771.
29. Wu, J.; Bondo, P. B.; Vuorinen, T.; Serianni, A. S. J. Am. Chem. Soc. 1992, 114, 3499-3505.
30. Junicke, H.; Serianni, A. S.; Steinborn, D. J. Org. Chem. 2000, 65, 4153-4161.
31. Botosoa, E. P.; Blumenstein, C.; MacKenzie, D. A.; Silvestre, V.; Remaud, G. S.; Kwiecień, R. A.; Robins, R. J. Anal. Biochem. 2009, 393, 182-188.