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70350458411
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-
note
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NAr mechanism. It is proposed that a small amount of dimethylamine is produced from the decomposition of DMF under these conditions and hence DMSO is a better solvent for such substrates.
-
-
-
-
40
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70350460548
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note
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+ 271.0917; found 271.0923.
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-
-
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41
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70350454451
-
-
note
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+ 297.0709; found 297.0712.
-
-
-
-
42
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70350446282
-
-
note
-
4). Subsequent filtration and concentration yielded a crude oil, which was purified by flash chromatography [hexane/EtOAc, 7:3] to afford the desired product.
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