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34249800711
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The relative stereochemistry of the newly created stereocenter was determined by NOESY experiments over compounds 8a and 9a see Supporting Information
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The relative stereochemistry of the newly created stereocenter was determined by NOESY experiments over compounds 8a and 9a (see Supporting Information).
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38
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34249803626
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A solvent study over substrate 7a was performed (with the process under microwave irradiation). The reaction was carried out in DCM, toluene, THF, and acetonitrile. The best results in terms of selectivity and yield were obtained in DCM.
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A solvent study over substrate 7a was performed (with the process under microwave irradiation). The reaction was carried out in DCM, toluene, THF, and acetonitrile. The best results in terms of selectivity and yield were obtained in DCM.
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