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Crystal data for 3-H: C34H35BN2 · C6D5Br, MW, 6.44.46, mono-clinic, space group P21/n, a, 12.230(5, b, 14864(4, c, 18.248(7) Å, β, 97.255(15)°, V, 3291(2) Å3, Z, 4, p, 1.291 gcm-3, MoKα radiation, γ, 0.71073 Å, T, 173(2) K, 5650 measured reflections, 4602 unique, min/max transmission, 0.666629 and 0.8615, I > σ, 0.0502, wR, 0.1277, GoF, 1.050, No. of parameters, 403, final difference map within, 0.59 and, 1.32 e Å3. Crystal data for 4-H: C34H35BN2O 2, MW, 514.45, monoclinic, space group P21/n, a, 1111.5020(3, b, 19.5600(7, c, 13.6530(5) Å β, 111114.3910(19)°, V, 2797.49(16) Å3, Z, 4, p, 1
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