Microwave synthesis in process chemistry method, scale and scope

Chimica Oggi

Volumn 27, Issue 2, 2009, Pages 6-10

  Moseley, Jonathan D ^a  

^a ASTRAZENECA   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 67649840870     PISSN: 0392839X     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (46)

1. C. O. Kappe, A. Stadler, Microwaves in Organic and Medicinal Chemistry, Wiley-VCH, Weinheim (2005).
2. nd Edn. (Ed.; A. Loupy), Wiley-VCH, Weinheim (2006)
3. (b) Microwave Assisted Organic Synthesis, (Eds.: J. P. Tierney, P. Lidstrom), Blaclwell, Oxford (2005)
4. (c) B. L. Hayes, Microwave Synthesis: Chemistry at the Speed of Light, CEM, Matthews (2002).
5. (a) C. O. Kappe, Angew. Chem. Int. Ed. 43, pp. 6250-6284 (2004) ;
6. (b) B. L. Hayes, Aldrichimica Acta 37, pp. 66-76 (2004) ;
7. (c) M. Nuchter, B. Ondruschka et al., Green Chem. 6, pp. 128-141 (2004).
8. B. A. Roberts, C. R. Strauss, Acc. Chem. Res. 38, pp. 653-661 (2005).
9. C. Gabriel, S. Gabriel et al., Chem. Soc. Rev. 27, pp. 213-223 (1998).
10. M. D. Bowman, J. L Holcomb et al., Org. Process Res. Dev. 12, pp. 41-57 (2008).
11. See relevant sections in references 1-3.
12. For selected examples see:- (a) W. S. Bremner, M. G. Organ, J. Comb. Chem. 9, pp. 14-16 (2007)
13. (b) I. R. Baxendale, M. R. Pitts, Chemistry Today 24 (3), pp. 41-45 (2006)
14. (c) M. C. Bagley, R. L. Jenkins et al., J. Org. Chem. 70, pp. 7003-7006 (2005)
15. (d) N. S. Wilson, C. R. Sarko et al., Org. Process Res. Dev. 8, pp. 535-538 (2004)
16. (e) W.-C. Shieh, M. Lozanov et al., Tetrahedron Lett. 44, pp. 6943-6945 (2003)
17. (f) W.-C. Shieh, S. Dell et al., Tetrahedron left. 43, pp. 5607-5609 (2002)
18. (g) B. M. Khadilkar, V. R. Madyar, Org. Process Res. Dev. 5, pp. 452-455 (2001)
19. (h) J. Marquie, G. Salmoria et al., Ind. Eng. Chem. Res. 40, pp. 4485-4490 (2001).
20. (a) S. Horikoshi, T. Hamamura et al., Org. Process Res. Dev. 12, pp. 1089-1093 (2008)
21. (b) S. Horikoshi, S. lida et al., Org. Process Res. Dev. 12, pp. 257-263 (2008).
22. st January 2009.
23. (a) www.anton-paar.com;
24. (b) www.biotage.com;
25. (c) www.cem.com;
26. (d) www.milestonesrl.com.
27. J. M. Kremsner, A. Stadler et al., Top. Curr. Chem. 266, pp. 233-278 (2006).
28. J. D. Moseley, P. Lenden et al., Org. Process Res. Dev. 12, pp. 30-40 (2008).
29. (a) J. Alcazar, G. Diels et al., QSAR Comb. Sci. 23, pp. 906-910 (2004) ;
30. (b) A. Stadler, B. H. Yousefi et al., Org. Process Res. Dev. 7, pp. 707-716 (2003).
31. G. C. Lloyd-Jones, J. D. Moseley et al., Synthesis, pp. 661-689 (2008).
32. J. D. Moseley, S. J. Lawton, Chimica Oggi/Chemistry Today 25 (2), pp. 16-19 (2007).
33. J. D. Moseley, R. F. Sankey et al., Tetrahedron 62, pp. 4685-4689 (2006).
34. J. D. Moseley, P. Lenden, Tetrahedron 63, pp. 4120-4125 (2007).
35. A. M. M. Castro, Chem. Rev. 104, pp. 2939-3002 (2004).
36. J. D. Moseley, E. K. Woodman, Org. Process Res. Dev. 12, pp. 967-981 (2008).
37. (a) T. M. Barnard, G. S. Vanier et al., Org. Process Res. Dev. 10, pp. 1233-1237 (2006) ;
38. (b) N. E. Leadbeater, V. A. Williams et al., Synlett. pp. 2953-2958 (2006)
39. (c) N. E. Leadbeater, V. A. Williams et al., Org. Process Res. Dev. 10, pp. 833-837 (2006).
40. (a) I. Beletskaya, A. Cheprakov, Chem. Rev. 100, pp. 309-3066 (2000)
41. (b) V. Farina, Adv. Synth. Catal. 346, pp. 1553-1582 (2004).
42. T. M. Glasnov, H. Tye et al., Tetrahedron 64, pp. 2035-2041 (2008).
43. N. E. Leadbeater, J. R. Schmink, Tetrahedron 63, pp. 6764-6773 (2007).
44. J. P. Gilday, P. Lenden et al., J. Org. Chem. 73, pp. 3130-3134 (2008).
45. J. D. Moseley, R. L. Woodward, unpublished results.
46. J. M. Kremsner, C. O. Kappe, Eur. J. Org. Chem., pp. 3672-3679 (2005).