Determination of multi-class pesticides in wines by solid-phase extraction and liquid chromatography-tandem mass spectrometry

Journal of Chromatography A

Volumn 1216, Issue 31, 2009, Pages 5856-5867

  Economou, Anastasios ^a   Botitsi, Helen ^a   Antoniou, Spyros ^a   Tsipi, Despina ^a  

^a General Chemical State Laboratory   (Greece)

Author keywords

Liquid chromatography; Pesticides; SPE; Tandem mass spectrometry; Wines

Indexed keywords

AVERAGE RECOVERY; BENOMYL; CARBARYL; CARBENDAZIM; CHEMICAL CLASS; CONCENTRATION LEVELS; ELECTROSPRAY; ION TRANSITION; IONISATION; LC-MS/MS; LIMIT OF QUANTIFICATIONS; LIMITS OF DETECTION; LIMITS OF QUANTIFICATION; LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY; MATRIX EFFECTS; METHOD VALIDATIONS; MULTI-CLASS; RELATIVE STANDARD DEVIATIONS; SAMPLE CLEAN-UP; SELECTED REACTION MONITORING; SINGLE-STEP; SOLID-PHASE EXTRACTION; SPE; TANDEM MASS SPECTROMETRY; TARGET COMPOUND; TARGET SPECIES; TRANSFORMATION PRODUCTS; WINE SAMPLE;

AGRICULTURAL CHEMICALS; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; ELECTROSPRAY IONIZATION; LIQUIDS; MASS SPECTROMETERS; MASS SPECTROMETRY; PESTICIDES; SOLAR RADIATION; SOLVENT EXTRACTION; SPECTRUM ANALYSIS; WINE;

HIGH PRESSURE LIQUID CHROMATOGRAPHY;

ALDICARB; AMITRAZ; BENOMYL; CARBARIL; CARBENDAZIM; CARBOFURAN; CHLORPROPHAM; DIMETHOATE; DISULFOTON; ENILCONAZOLE; ETHIOFENCARB; FLUSILAZOLE; METALAXYL; METHIOCARB; METHOMYL; MYCLOBUTANIL; PESTICIDE; PIRIMICARB; PROCHLORAZ; PROPICONAZOLE; PROPOXUR; THIOPHANATE METHYL; TIABENDAZOLE; TRIADIMEFON; TRIAZOPHOS;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; CONTROLLED STUDY; ELECTROSPRAY MASS SPECTROMETRY; FOOD CONTAMINATION; FOOD SAFETY; LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; TOXIN ANALYSIS; WINE;

BENZIMIDAZOLES; CARBAMATES; CARBARYL; CHROMATOGRAPHY, LIQUID; LINEAR MODELS; PESTICIDES; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; THIOPHANATE; WINE;

EID: 67649792090     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2009.06.031     Document Type: Article

References (28)

1. Cabras P., and Conte E. Food Addit. Contam. 18 (2001) 880
2. Off. J. Eur. Union L70 March (2005) 1
3. Off. J. Eur. Union L58 March (2008) 1
4. http://www.awri.com.au/agrochemicals/mrls/
5. Avramides E.J., Lentza-Rizos Ch., and Mojacevic M. Food Addit. Contam. 20 (2003) 699
6. Cambras P., and Angioni A. J. Agric. Food Chem. 48 (2000) 967
7. http://agriculture.gouv.fr/IMG/pdf/enqueteraisin.pdf
8. http://www.pan-europe.info/Resources/Briefings/Message_in_a_bottle_Resul ts.pdf
9. Flamini R., and Panighel A. Mass Spectrom. Rev. 25 (2006) 741
10. Alder L., Greulich K., Kempe G., and Vieth B. Mass Spectrom. Rev. 25 (2006) 838
11. Cunha S.C., Fernandes J.O., Alves A., and Oliveira M.B.P.P. J. Chromatogr. A 1216 (2009) 119
12. Patil S.H., Banerjee K., Dasgupta S., Oulkar D.P., Patil S.B., Jadhav M.R., Savant R.H., Adsule P.G., and Deshmukh M.B. J. Chromatogr. A 1216 (2009) 2307
13. Wong J.W., Webster M.G., Halverson C.A., Hengel M.J., Ngim K.K., and Ebeler S.E. J. Agric. Food Chem. 51 (2003) 1148
14. Pang G.F., Fan C.L., Liu Y.M., Cao Y.Z., Zhang J.J., Fu B.L., Li X.M., Li Z.Y., and Wu Y.P. Food Addit. Contam. 23 (2006) 777
15. Wu J., Tragas C., Lord H., and Pawliszyn J. J. Chromatogr. A 976 (2002) 357
16. Goto T., Ito Y., Oka H., Saito I., Matsumoto H., Sugiyama H., Ohkubo C., Nakazawa H., and Nagase H. Anal. Chim. Acta 531 (2005) 79
17. Nozal M.J., Bernal J.L., Jimenez J.J., Marti{dotless}n M.T., and Bernal J. J. Chromatogr. A 1076 (2005) 90
18. Plaza Bolãnos P., Romero-González R., Garrido Frenich A., and Martínez Vidal J.L. J. Chromatogr. A 1208 (2008) 16
19. Payá P., Anastassiades M., Mack D., Sigalova I., Tasdelen B., Oliva J., and Barba A. Anal. Bioanal. Chem. 389 (2007) 1697
20. Trösken E.R., Bittner N., and Völkel W. J. Chromatogr. A 1083 (2005) 113
21. European Commission, DG-SANCO, Method validation and quality control procedures for pesticide residues analysis in food and feed, Document No. SANCO/3131/2007, Brussels, October, 2007.
22. Botitsi H., Economou A., and Tsipi D. Anal. Bioanal. Chem. 389 (2007) 1685
23. Roberts T., and Hutson D. Metabolic Pathways of Agrochemicals vol. II (1999), The Royal Society of Chemistry, Cambridge UK
24. Niessen W.M.A., Manini P., and Andreoli R. Mass Spectrom. Rev. 25 (2006) 881
25. Thompson M. Analyst 125 (2000) 2020
26. ISO/TS. 21748. Guide to the use of Repeatability Reproducibility and Trueness Estimates in Measurement Uncertainty Estimation (2004), International Organization for Standardization, Geneva
27. V.J. Barwick, L.R. Ellison, VAM Project 3.2.1. Development and harmonisation of measurement uncertainty principles. Part d: protocol for uncertainty evaluation from validation data. Report No: LGC/VAM/1998/088, 2000.
28. http://ec.europa.eu/sanco_pesticides/public/index.cfm (accessed 25 May 2009).