SCOPUS 정보 검색 플랫폼

European Journal of Inorganic Chemistry

Volumn , Issue 17, 2009, Pages 2508-2511

Synthesis, structure and catalysis of tetranuclear copper(II) open cubane for henry reaction on water

(2) Jammi, Suribabu a Punniyamurthy, Tharmalingam a

a INDIAN INSTITUTE OF TECHNOLOGY GUWAHATI (India)

Author keywords

C C bond formation; Copper; Henry reaction; Heterogeneous catalysis; Water

Indexed keywords

COPPER COMPOUNDS;

C-C BOND FORMATION; CATALYSE; CUBANES; HENRY REACTIONS; HIGHER YIELD; SYNTHESISED;

CATALYSIS;

EID: 66549085002 PISSN: 14341948 EISSN: 10990682 Source Type: Journal
DOI: 10.1002/ejic.200900141 Document Type: Article

Times cited : (35)

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- X-ray data were collected with a Bruker SMART APEX equipped with a CCD area detector using Mo-Kα radiation in the scan range 1.30° <θ < 27.96°. The structure was solved using SHELXL-97 (Göttingen, Germany, C144H216Cu8N 8O21, M, 2903.57, monoclinic, space group P2 1/c, a, 14.868(3) A, b, 29.556(5) Å, c, 18.797(3) Å, α, 90.00°, β, 101.441(9)°, y, 90.00°, V, 8096(2) Å3, Z, 2, T, 296(2) K, μ (λ, 0.71073 Å, 1.089 mm-1, dcaled= 1.191 Mg/m3, 99235 reflections measured, 18024 unique [Rint, 0.1383, R1, 0.0743, wR2, 0.1896 [1 > 2σ(l, R1, 0.2304, wR2, 0.2388 all data, GOF, 0.996
- 2 = 0.2388 (all data), GOF = 0.996.

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