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Volumn 4, Issue 2, 2009, Pages 314-320

Synthesis, structure, and application of self-assembled copper(II) aqua complex by H-bonding for acceleration of the nitroaldol reaction on water

Author keywords

C C coupling; Heterogeneous catalysis; Hydrogen bonds; Nitroaldol reaction; Self assembly

Indexed keywords

AQUA COMPLEXES; AQUA LIGANDS; BOND INTERACTIONS; C-C COUPLING; COMPLEX 1; H BONDINGS; HETEROGENEOUS CATALYSIS; NITROALDOL REACTION; ONE-POT SYNTHESIS; PENTACOORDINATED; SELF-ASSEMBLED; SQUARE-PYRAMIDAL GEOMETRIES; TECHNOLOGICAL PROCESS; X-RAY ANALYSIS;

EID: 59349098013     PISSN: 18614728     EISSN: 1861471X     Source Type: Journal    
DOI: 10.1002/asia.200800339     Document Type: Article
Times cited : (46)

References (72)
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    • During purification on silica gel column chromatography using CH 2Cl2/MeOH (9:1, complex 1 underwent crystallization whose X-ray data were collected on a Bruker SMART APEX equipped with a CCD area detector using Mo-Ku radiation in the scan range 1.20°-28.31°. C17H23CuNO5, Mr, 384.90, monoclinic, space group P21/c, a, 17.175(10, b, 10.451(6, c= 10.449(6) Å α, 90°, β;= 98.769(4)° ã, 90°, K, 1853.76(19) Aring;3, Z, 4, Dcalc, 1.379 Mg/m3, T= 296(2) K, crystal size 0.48 × 0.24 × 0.10mm3; 23855 reflections, 4340 unique reflections; (I>2σ(I, R1 =0.0810, wR2=0.3409, all data, GOF on F2, 2.501. The structure is solved by direct method using SHELXL-97 Göltingen. Germany. CCDC 705157 contains the supplementary crystallography data for this paper. These data can be obtained free of charge from The C
    • 3, Z = 4, Dcalc = 1.379 Mg/m3, T= 296(2) K, crystal size 0.48 × 0.24 × 0.10mm3; 23855 reflections, 4340 unique reflections; (I>2σ(I)); R1 =0.0810, wR2=0.3409, (all data), GOF (on F2) = 2.501. The structure is solved by direct method using SHELXL-97 Göltingen. Germany. CCDC 705157 contains the supplementary crystallography data for this paper. These data can be obtained free of charge from The Cambridge Cryslallographic Data Centre at www.ccdc.cam.ac.uk/data-request/cif.
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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.