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66149176853
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The chloride complex 1a was isolated as an orange powder that was proved to be a 57:43 mixture of two conformational isomers, and the bromide complex 1b isolated was a 90:10 mixture of two conformers. The iodide complex 1c was isolated as a single conformer.
-
The chloride complex 1a was isolated as an orange powder that was proved to be a 57:43 mixture of two conformational isomers, and the bromide complex 1b isolated was a 90:10 mixture of two conformers. The iodide complex 1c was isolated as a single conformer.
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-
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37
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66149179056
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-
The dihedral angle between the two Pd-square planes is approximately 40°. CCDC-718690 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/ retrieving.html (or from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB21EZ, UK; fax: (+44)1223-336-033; or deposit@ccdc.cam.ac.uk).
-
The dihedral angle between the two Pd-square planes is approximately 40°. CCDC-718690 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/ retrieving.html (or from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB21EZ, UK; fax: (+44)1223-336-033; or deposit@ccdc.cam.ac.uk).
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38
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0034104304
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For representative papers dealing with asymmetric ring-opening reactions of oxabenzonorbornadienes and azabenzonorbornadienes, see: (a) Lautens, M.; Renaud, J.-L.; Hiebert, S. J. Am. Chem. Soc. 2000, 122, 1804-1805.
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66149189246
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Carretero and co-workers generated cationic Pd complexes by treatment of palladium chloride complexes with NaB(ArF)4 or AgPF 6 and demonstrated their high catalytic activities in alkylative ring opening of oxabenzonorbornadienes and azabenzonorbornadienes. See refs 9d and 9e
-
6 and demonstrated their high catalytic activities in alkylative ring opening of oxabenzonorbornadienes and azabenzonorbornadienes. See refs 9d and 9e.
-
-
-
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47
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66149164372
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31P NMR (161 MHz) δ-3.62
-
31P NMR (161 MHz) δ-3.62
-
-
-
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48
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66149161699
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A monocationic species was probably generated in the latter case
-
A monocationic species was probably generated in the latter case.
-
-
-
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49
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66149182926
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In order to confirm the existence of a dimeric palladium species throughout the course of the reaction, we carried out the reaction in toluened8 using a stoichiometric amount of 1c/AgOTf 1:2, After the mixture was kept at 80 °C for 0.5 h, NaI was added. The 1H and 31P NMR spectra of the mixture showed almost the same signals as those of dimeric complex 1c
-
31P NMR spectra of the mixture showed almost the same signals as those of dimeric complex 1c.
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