Multiresidue pesticide analysis of wines by dispersive solid-phase extraction and ultrahigh-performance liquid chromatography-tandem mass spectrometry

Journal of Agricultural and Food Chemistry

Volumn 57, Issue 10, 2009, Pages 4019-4029

  Zhang, Kai ^a   Wong, Jon W ^a   Hayward, Douglas G ^a   Sheladia, Piyush ^b   Krynitsky, Alexander J ^a   Schenck, Frank J ^a   Webster, Michael G ^c   Ammann, Jeffrey A ^c   Ebeler, Susan E ^d  

^a CENTER FOR DRUG EVALUATION AND RESEARCH   (United States)

^b UNIVERSITY OF MARYLAND   (United States)

^c Alcohol and Tobacco Tax and Trade Bureau   (United States)

^d UNIVERSITY OF CALIFORNIA   (United States)

Author keywords

Multiresidue pesticide analysis; UPLC MS MS; Wines

Indexed keywords

PESTICIDE RESIDUE;

ARTICLE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; METHODOLOGY; QUALITY CONTROL; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; WINE;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; PESTICIDE RESIDUES; QUALITY CONTROL; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; WINE;

EID: 66149105802     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf9000023     Document Type: Article

References (37)

1. 2007 California Wine Sales Continue Increase, As Wine Expands Its Popularity Among Americans; California Wine Institute, 2007; found at http://www.wineinstitute.org/resources/statistics/articlel22.
2. Cabras, P.; Angioni, A. Pesticide residues in grapes, wine, and their processing products. J. Agric. Food Chem. 2000, 48, 967-973.
3. Flamini, R.; Panighel, A. Mass spectrometry in grape and wine chemistry. Part II: the consumer protection. Mass Spectrom. Rev. 2006, 25, 741-774.
4. Holland, P. T.; McNaughton, D. E.; Malcolm, C. P. Multiresidue analysis of pesticides in wines by solid-phase extraction. J. AO AC Int. 1994, 77, 79-86.
5. Miyake, Y.; Koji, K.; Matsuki, H.; Tajima, R.; Ono, M.; Mine, T. Fate of agrochemical residues, associated with malt and hops, during brewing. J. Am. Soc. Brew. Chem. 1999, 57, 46-54.
6. Prieto, A.; Ettiene, G.; Medina, D.; Buscéma, I.; Gonzalez, G.; Araujo, L. Analysing organophosphorus pesticides in wines using graphitized carbon black extraction cartridges. Food Addit. Contam. 1999, 70, 57-61.
7. Correia, M.; Delerue-Matos, C.; Alves, A. Multi-residue methodology for pesticide screening in wines. J. Chromatogr., A 2000, 889, 59-67.
8. Soleas, G. J.; Yan, J.; Hom, K.; Goldberg, D. M. Multiresidue analysis of seventeen pesticides in wine by gas chromatography with mass-selective detection. J. Chromatogr., A 2000, 552, 205-212.
9. Jiménez, J. J.; Bernal, J. L.; del Nozal, M. J.; Toribio, L.; Arias, E. Analysis of pesticide residues in wine by solid-phase extraction and gas chromatography with electron capture and nitrogen-phosphorus detection. J. Chromatogr., A 2001, 919, 147-156.
10. Miyake, Y.; Hashimoto, K.; Matsuki, H.; Ono, M.; Tajima, R. Fate of insecticide and fungicide residues on barley during storage and malting. J. Am. Soc. Brew. Chem. 2002, 60, 110-115.
11. Wong, J. W.; Webster, M. G.; Halverson, C. A.; Hengel, M. J.; Ngim, K. K.; Ebeler, S. E. Multiresidue pesticide analysis in wines by solid-phase extraction and capillary gas chromatography-mass spectrometric detection with selective ion monitoring. J. Agrie. Food Chem. 2003, 57, 1148-1161.
12. Wong, J. W.; Webster, M. G.; Bezabeh, D. Z.; Hengel, M. J.; Ngim, K. K.; Krynitsky, A. J.; Ebeler, S. E. Multiresidue determination of pesticides in malt beverages by capillary gas chromatography with mass spectrometry and selected ion monitoring. J. Agric. Food Chem. 2004, 52, 6361-6372.
13. Albero, B.; Sánchez-Brunete, C.; Tadeo, J. L. Multiresidue determination of pesticides in juice by solid-phase extraction and gas chromatography-mass spectrometry. Talanta 2005, 66, 917-924.
14. Chu, X. G.; Hu, X. Z.; Yao, H. Y. Determination of 266 pesticide residues in apple juice by matrix solid-phase dispersion and gas chromatography-mass selective detection. J. Chromatogr., A 2005, 7005, 201-210.
15. Goto, T.; Ito, Y.; Oka, H.; Saito, I.; Matsumoto, H.; Sugiyama, H.; Ohkubo, C.; Nakazawa, H.; Nagase, H. The high throughput analysis of N-methyl carbamate pesticides in wine and juice by electrospray ionization liquid chromatography tandem mass spectrometry with direct sample injection into a short column. Anal. Chim. Acta 2005, 531, 79-86.
16. Trösken, E. R.; Bittner, N.; Völkel, W. Quantitation of 13 azole fungicides in wine samples by liquid chromatography-tandem mass spectrometry. J. Chromatogr., A 2005,1083, 113-119.
17. Omote, M.; Harayama, K.; Sasaki, T.; Mochizuki, N.; Yamashita, H. Analysis of simultaneous screening for 277 pesticides in malt and beer by liquid chromatography with tandem mass spectrometry. J. Am. Soc. Brewing Chem. 2006, 64, 139-150.
18. Pang, G.-F.; Fan, C-L.; Liu, Y.-M.; Cao, Y.-Z.; Zhang, J.-J.; Fu, B.-L.; Li, X.-M.; Li, Z.-Y.; Wu, Y.-P. Multi-residue method for the determination of 450 pesticide residues in honey, fruit juice and wine by double cartridge solid-phase extraction/gas chromatographymass spectrometry and liquid chromatography-tandem mass spectrometry. Food Addit. Contam. 2006, 23, 777-810.
19. Gilbert-López, B.; Garcia-Reyes, J. F.; Mezcua, M.; Molinia-Diaz, A.; Fernández-Alba, A. R. Determination of postharvest fungicides in fruit juices by solid-phase extraction followed by liquid chromatography time-of-flight mass spectrometry. J. Agrie. Food Chem. 2007, 55, 10547-10556.
20. Jezussek, M.; Münch, F.; Gilsbach, W. Bestimmung von pestizidrückständen in wein mittels LC-MS/MS-direkte messung im vergleich zu zwei aufarbeitungsmethoden (LC-MS/MS determination of pesticide residues in wine-comparison of direct measurement with two work-up procedures). Dtsch. Lebensm.-Rundsch. 2007,103, 405-411.
21. Paya, P.; Anastassiades, M.; Mack, D.; Sigalova, I.; Tasdelen, B.; Oliva, J.; Barba, A. Analysis of pesticide residues using the Quick Easy Cheap Effective Rugged and Safe (QuEChERS) pesticide multiresidue method in combination with gas and liquid chromatography and tandem mass spectrometric detection. Anal. Bioanal. Chem. 2007,559, 1697-1714.
22. Romero-González, R.; Garrido-Frenich, A.; Martinez Vidal, J. L. Multiresidue method for fast determination of pesticides in fruit juices by ultra performance liquid chromatography coupled to tandem mass spectrometry. Talanta 2008, 76, 211-225.
23. Swartz, M. E. UPLC™: an introduction and review. J. Liq. Chromatogr. Mat. Technol. 2005, 28, 1253-1263.
24. Fillion, J.; Sauve, F.; Selwyn, J. Multiresidue method for the determination of residues of 251 pesticides in fruits and vegetables by gas chromatography/mass spectrometry and liquid chromatography with fluorescence detection: chromatographic pesticide residue analysis. J. AO AC Int. 2000, 83, 698-713.
25. Anastassiades, M.; Lehotay, S. J.; Štajnbaher, D.; Schenck, F. J. Fast and easy multiresidue method employing acetonitrile extraction/ partitioning and "dispersive solid-phase extraction" for the determination of pesticide residues in produce. J. AO AC Int. 2003,86,412-431.
26. Pang, G. F.; Fan, C. L.; Liu, Y. M.; Cao, Y. Z.; Zhang, J. J.; Li, X. M.; Li, Z. Y.; Wu, Y. P.; Guo, T. T. Determination of residues of 446 pesticides in fruits and vegetables by three-cartridge solid-phase extraction-gas chromatography-mass spectrometry and liquid chromatography-tandem mass spectrometry. J. AO AC Int. 2006, 59, 740-771.
27. Okihashi, M.; Kitagawa, Y.; Akutsu, K.; Obana, H.; Tanaka, Y. Rapid method for the determination of 180 pesticide residues in foods by gas chromatography/mass spectrometry and flame photometric detection. J. Pestic. Sci. 2005, 30, 368-377.
28. Lehotay, S. J.; de Kok, A.; Hiemstra, M.; Van Bodegraven, P. Validation of a fast and easy method for the determination of residues from 229 pesticides in fruits and vegetables using gas and liquid chromatography and mass spectrometric detection. J. AO AC Int. 2005, 55, 595-614.
29. Shimelis, O.; Yang, Y.; Stenerson, K.; Kaneko, T.; Ye, M. Evaluation of a solid-phase extraction dual-layer carbon/primary secondary amine for clean-up of fatty acid matrix components from food extracts in multiresidue pesticide analysis. J. Chromatogr., A 2007, 1165,18-25.
30. Mol, H. G. J.; Rooseboom, A.; van Dam, R.; Roding, M.; Arondeus, K.; Sunarto, S. Modification and re-validation of the ethyl acetatebased multi-residue method for pesticides in produce. Anal. Bioanal. Chem. 2007, 559, 1715-1754.
31. Kovalczuk, T.; Jech, M.; Poustka, J.; Hajšlová, J. Ultra-performance liquid chromatography-tandem mass spectrometry: A novel challenge in multiresidue pesticide analysis in food. Anal. Chim. Acta 2006, 577, 8-17.
32. Leandro, C. C.; Hancock, P.; Fussell, R. J.; Keely, B. J. Comparison of ultra-performance liquid chromatography and high-performance liquid chromatography for the determination of priority pesticides in baby foods by tandem quadrupole mass spectrometry. J. Chromatogr., A 2006, 1103, 94-101.
33. Gilbert-López, B.; García-Reyes, J. F.; Ortega-Barrales, P.; MolinaDiaz, A.; Fernández-Alba, A. R. Analyses of pesticide residues in fruit-based baby food by liquid chromatography/electrospray ionization time-of-flight mass spectrometry. Rapid Commun. Mass Spectrom. 2007, 27, 2059-2071.
34. EC Council Directive 2002/657/EC of 12 August, 1990 on implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Off. J. Eur. Communities 2002, L221/8.
35. Ortelli, D.; Edder, P. Survey of pesticide residues in Swiss and foreign wines. Mitt. Lebensmittelunters. Hyg. 2005, 96, 311-320; http:// www.bag.admin.ch/dokumentation/publikationen/02212/index. html?lang = de#.
36. European Council Directives 76/895/EEC, 86/362/EEC, 86/363/ EEC, and 90/642/EEC.
37. Protection of the Environment. Code of Federal Regulations; Parts 150-189, Title 40; Office of the Federal Register, U.S. National Archives and Records Administration, U.S. Government Printing Office: Washington, DC, 2007.