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Crystal data for [1](BF4)4 2acetone: G 94H124N12B4F16Ni 4, O2, monoclinic, P21/n, a= 16.368(2) Å, b, 16.892(2) Å, c, 18.687(3) Å, β, 100.086(2)°, V, 5087.2(12) Å3, Z, 2, T, 153(2) K, Dcalcd, 1-329 g cm-3, R(F, 0.0959 for 5168 observed intensities (1 ≥ 2σT, collected in the range 3.1° ≤ 2θ ≤ 51.7°. The asymmetric unit contains two acetone molecules, one of which is disordered. The nondisordered acetone molecule is located inside the molecular rectangle. Crystal data for [3a, C16H19N2BrNi, orthorhombic, P2 12121 a, 10.2497(4) Å, b, 10.7909(5) Å, c, 14.1980(6) Å, V, 1570.35(12) Å3, Z, 4
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2 and one disordered water molecule.
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