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The role of hydrogen bonding in the stabilization of the solid-state structure of aqua-transition metal complexes has long been recognized: (a) Rochon, F. D.; Melanson, R. Inorg. Chem. 1987, 26, 989. (b) Britten, J. F.; Lippert, B.; Lock, C. J.; Pilon, P. Inorg. Chem. 1982, 21, 1936. (c) Hollis, L. S.; Lippard, S. J. Inorg. Chem. 1983, 22, 2605. (d) Brown, I. D. Structure and Bonding in Crystals; Academic Press: New York, 1981; Vol. II. (e) Braga, D.; Grepioni, F. Acc. Chem. Res. 1994, 27, 51. (f) Braga, D.; Grepioni, F.; Sabatino, P.; Desiraju, G. R. Organometallics 1994, 13, 3532.
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The role of hydrogen bonding in the stabilization of the solid-state structure of aqua-transition metal complexes has long been recognized: (a) Rochon, F. D.; Melanson, R. Inorg. Chem. 1987, 26, 989. (b) Britten, J. F.; Lippert, B.; Lock, C. J.; Pilon, P. Inorg. Chem. 1982, 21, 1936. (c) Hollis, L. S.; Lippard, S. J. Inorg. Chem. 1983, 22, 2605. (d) Brown, I. D. Structure and Bonding in Crystals; Academic Press: New York, 1981; Vol. II. (e) Braga, D.; Grepioni, F. Acc. Chem. Res. 1994, 27, 51. (f) Braga, D.; Grepioni, F.; Sabatino, P.; Desiraju, G. R. Organometallics 1994, 13, 3532.
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The role of hydrogen bonding in the stabilization of the solid-state structure of aqua-transition metal complexes has long been recognized: (a) Rochon, F. D.; Melanson, R. Inorg. Chem. 1987, 26, 989. (b) Britten, J. F.; Lippert, B.; Lock, C. J.; Pilon, P. Inorg. Chem. 1982, 21, 1936. (c) Hollis, L. S.; Lippard, S. J. Inorg. Chem. 1983, 22, 2605. (d) Brown, I. D. Structure and Bonding in Crystals; Academic Press: New York, 1981; Vol. II. (e) Braga, D.; Grepioni, F. Acc. Chem. Res. 1994, 27, 51. (f) Braga, D.; Grepioni, F.; Sabatino, P.; Desiraju, G. R. Organometallics 1994, 13, 3532.
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35
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85087582967
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note
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2] in 90% yield. See also ref 6a for another method of preparation of this complex.
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36
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0003872738
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Ibers, J. A., Hamilton, W. C., Eds.; Kynoch Press: Birmingham, U.K.
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Cromer, D. T.; Waber, J. T. In International Tables for X-ray Crystallography; Ibers, J. A., Hamilton, W. C., Eds.; Kynoch Press: Birmingham, U.K., 1974.
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International Tables for X-ray Crystallography
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Waber, J.T.2
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