Fluidized bed chemical vapor deposition of pyrolytic carbon - I. Effect of deposition conditions on microstructure

Carbon

Volumn 47, Issue 2, 2009, Pages 396-410

  Lopez Honorato E ^a   Meadows, P J ^a   Xiao, P ^a  

^a UNIVERSITY OF MANCHESTER   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

ACETYLENE; FLUID DYNAMICS; FLUIDIZATION; FLUIDIZED BED PROCESS; FLUIDIZED BEDS; LIGHTING; LOW PRESSURE CHEMICAL VAPOR DEPOSITION; MICROSTRUCTURE; RAMAN SCATTERING; RAMAN SPECTROSCOPY; SPECTRUM ANALYSIS; VAPORS;

DEPOSITION CONDITIONS; DEPOSITION PROCESSES; DEPOSITION TEMPERATURES; DOMAIN SIZES; FLUIDIZED BED CHEMICAL VAPOR DEPOSITIONS; NUCLEATION MECHANISMS; POROSIMETRY; PRECURSOR CONCENTRATIONS; PYROLYTIC CARBONS; X-RAY DIFFRACTIONS;

DEPOSITION;

EID: 57849169477     PISSN: 00086223     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.carbon.2008.10.023     Document Type: Article

References (51)

1. Guellali M., Oberacker R., and Hoffmann M.J. Influence of the matrix microstructure on the mechanical properties of CVI-infiltrated carbon fiber felts. Carbon 43 9 (2005) 1954-1960
2. Carrere N., Lardillier F., Vidal-Sétif M.-.H., and Valle R. Influence of microstructure of pyrocarbon coating on mechanical properties of SiC/Ti6242 composite. Mater Sci Technol 19 (2003) 669-675
3. Basu R.N., Altin O., Mayo M.J., Randall C.A., and Eser S. Pyrolytic carbon deposition on porous cathode tubes and its use as an interlayer for solid oxide fuel cell zirconia electrolyte fabrication. J Electrochem Soc 148 5 (2001) A506-A512
4. Ma L., and Sines G. High resolution, structural studies of a pyrolytic carbon used in medical applications. Carbon 40 3 (2002) 451-454
5. Dayton R.W., Oxley J.H., and Townley C.W. Ceramic coated particle nuclear fuels. J Nucl Mater 11 1 (1964) 1-31
6. Martin D.G. Considerations pertaining to the achievement of high burn-ups in HTR fuel. Nucl Eng Des 213 (2002) 241-258
7. Je J.H., and Lee J.Y. The cause of size difference. Soot particles and the growth features of Isotropic pyrolytic carbon. Carbon 25 4 (1987) 586
8. Shi R., Li H.J., Yang Z., and Kang M.K. Deposition mechanism of pyrolytic carbons at temperature between 800 and 1200 °C. Carbon 35 12 (1997) 1789-1792
9. Ford L.H., and Bilsby C.F. Porosity related to structure for low temperature propylene pyrocarbons. J Nucl Mater 60 1 (1976) 79-88
10. Luhleich H., Seeberger D., Koizlik K., and Nickel H. Two-component model of pyrocarbon and its effect on material parameter analysis. J Vac Sci Technol 12 4 (1975) 750-753
11. Koizlik K., Linke J., Luhleich H., and Nickel H. Some theoretical aspects of pyrocarbon formation in the gas phase during hydrocarbon pyrolysis. Thin Solid Films 40 (1977) 115-121
12. Grisdale R.O. The formation of black carbon. J Appl Phys 24 9 (1953) 1082-1091
13. Monthioux M., Allouche H., and Jacobsen R.L. Chemical vapour deposition of pyrolytic carbon on carbon nanotubes: Part 3: growth mechanisms. Carbon 44 15 (2006) 3183-3194
14. Kaae J.L. The mechanism of the deposition of pyrolytic carbons. Carbon 23 6 (1985) 665-673
15. Lavenac J., Langlais F., Bourrat X., and Naslain R. Deposition process of laminar pyrocarbon from propane. J Phys IV France 11 (2001) 1013-1021
16. Feron O., Langlais F., Naslain R., and Thebault J. On kinetic and microstructural transitions in the CVD of pyrocarbon from propane. Carbon 37 9 (1999) 1343-1353
17. Feron O., Langlais F., and Naslain R. Analysis of the gas phase by in situ FTIR spectrometry and mass spectrometry during the CVD of pyrocarbon from propane. Chem Vap Deposit 5 1 (1999) 37-47
18. Hu Z.J., and Hüttinger K.J. Mechanisms of carbon deposition - a kinetic approach. Carbon 40 4 (2002) 624-628
19. Hu Z.J., Zhang W.G., Huttinger K.J., Reznik B., and Gerthsen D. Influence of pressure, temperature and surface area/volume ratio on the texture of pyrolytic carbon deposited from methane. Carbon 41 4 (2003) 749-758
20. Dong G.L., and Huttinger K.J. Consideration of reaction mechanisms leading to pyrolytic carbon of different textures. Carbon 40 14 (2002) 2515-2528
21. Vignoles G.L., Langlais F., Descamps C., Mouchon A., Le Poche H., Reuge N., et al. CVD and CVI of pyrocarbon from various precursors. Surf Coat Technol 188-189 (2004) 241-249
22. Norinaga K., Deutschmann O., and Huttinger K.J. Analysis of gas phase compounds in chemical vapor deposition of carbon from light hydrocarbons. Carbon 44 9 (2006) 1790-1800
23. Oberlin A. Pyrocarbons. Carbon 40 1 (2002) 7-24
24. López-Honorato E., Meadows P.J., Xiao P., Marsh G., and Abram T.J. Structure and mechanical properties of pyrolytic carbon produced by fluidized bed chemical vapor deposition. Nucl Eng Des 238 11 (2008) 3121-3128
25. Lackey W.J., Stinton D.P., and Sease J.D. Improved gas distributor for coating high-temperature gas-cooled reactor fuel particles. Nucl Technol 35 (1977) 227-237
26. Li Z.Q., Lu C.J., Xia Z.P., Zhou Y., and Luo Z. X-ray diffraction patterns of graphite and turbostratic carbon. Carbon 45 (2007) 1686-1695
27. Bourrat X., Trouvat B., Limousin G., and Vignoles G. Pyrocarbon anisotropy as measured by electron diffraction and polarized light. J Mater Res 15 1 (2000) 92-101
28. Delle W., Koizlik K., Price M.S.T., and Wallura E. Quality control techniques for pyrocarbon. Nucl Technol 35 (1977) 284-292
29. Reznik B., and Hüttinger K.J. On the terminology for pyrolytic carbon. Carbon 40 4 (2002) 621-624
30. Pollmann E., Pelissier J., Yust C.S., and Kaae J.L. Transmission electron microscopy of pyrocarbon coatings. Nucl Technol 35 (1977) 301-309
31. Yust C.S., and Krautwasser H.P. Transmission electron microscopy of propene-derived pyrolytic carbon coatings. Carbon 13 2 (1975) 125-133
32. Lespade P., Marchand A., Couzi M., and Cruege F. Caracterisation de materiaux carbones par microspectrometrie Raman. Carbon 22 4-5 (1984) 375-385
33. Yoshida A., Kaburagi Y., and Hishiyama Y. Full width at half maximum intensity of the G band in the first order Raman spectrum of carbon material as a parameter for graphitization. Carbon 44 11 (2006) 2333-2335
34. Tuinstra F., and Koenig J.L. Raman spectrum of graphite. J Chem Phys 53 3 (1970) 1126-1130
35. Knight D., and White W.B. Characterization of diamond films by Raman spectroscopy. J Mater Res 4 2 (1989) 385-393
36. Bokros J.C. The structure of pyrolytic carbon deposited in a fluidized bed. Carbon 3 1 (1965) 17-20
37. Bard R.J., Baxman H.R., Bertino J.P., and O'Rourke J.A. Pyrolytic carbons deposited in fluidized beds at 1200 to 1400 °C from various hydrocarbons. Carbon 6 5 (1968) 603-606
38. Zickler G.A., Smarsly B., Gierlinger N., Peterlik H., and Paris O. A reconsideration of the relationship between the crystallite size La of carbons determined by X-ray diffraction and Raman spectroscopy. Carbon 44 15 (2006) 3239-3246
39. Warren B.E., and Bodenstein P. The diffraction pattern of fine particle carbon blacks. Acta Cryst 18 (1965) 282-286
40. Vander Wal R.L., Tomasek A.J., Street K., Hull D.R., and Thompson W.K. Carbon nanostructure examined by lattice fringe analysis of high-resolution transmission electron microscopy images. Appl Spectrosc 58 2 (2004) 230-237
41. Lespade P., Al-Jishi R., and Dresselhaus M.S. Model for Raman scattering from incompletely graphitized carbons. Carbon 20 5 (1982) 427-431
42. Castiglioni C., Tommasini M., and Giuseppe Z. Raman spectroscopy of polyconjugated molecules and materials: confinement effect in one and two dimensions. Phil Trans Royal Soc Lond A 362 (2004) 2425-2459
43. Jellison G.E., Hunn J.D., and Lowden R.A. Optical characterization of tristructural isotropic fuel particle cross-sections using generalized ellipsometry. J Nucl Mater 352 (2006) 6-12
44. Vander Wal R.L. Soot precursor carbonization: visualization using LIF and LII and comparison using bright and dark field TEM. Combust Flame 112 (1998) 607-616
45. De Pauw V., Kalhofer S., and Gerthsen D. Influence of the deposition parameters on the texture of pyrolytic carbon layers deposited on planar substrates. Carbon 42 2 (2004) 279-286
46. De Pauw V., Collin A., Send W., Hawecker J., Gerthsen D., Pfrang A., et al. Deposition rates during the early stages of pyrolytic carbon deposition in a hot-wall reactor and the development of texture. Carbon 44 14 (2006) 3091-3101
47. Vander Wal R.L., and Tomasek A.J. Soot nanostructure: dependence upon synthesis conditions. Combust Flame 136 1-2 (2004) 129-140
48. Coffin L.F. Structure-property relations for pyrolytic graphite. J Am Ceram Soc 47 10 (1964) 473-478
49. De Pauw V., Reznik B., Kalhofer S., Gerthsen D., Hu Z.J., and Huttinger K.J. Texture and nanostructure of pyrocarbon layers deposited on planar substrates in a hot-wall reactor. Carbon 41 1 (2003) 71-77
50. Becker A., and Huttinger K.J. Chemistry and kinetics of chemical vapor deposition of pyrocarbon-II pyrocarbon deposition from ethylene, acetylene and 1, 3-butadiene in the low temperature regime. Carbon 36 3 (1998) 177-199
51. Becker A., and Huttinger K.J. Chemistry and kinetics of chemical vapor deposition of pyrocarbon-III pyrocarbon deposition from propylene and benzene in the low temperature regime. Carbon 36 3 (1998) 201-211