Synthesis, structure, and magnetism of hexanuclear copper(II) phosphonates

Inorganic Chemistry

Volumn 47, Issue 20, 2008, Pages 9553-9560

  Chandrasekhar, Vadapalli ^a   Senapati, Tapas ^a   Sañudo, E Carolina ^b  

^a INDIAN INSTITUTE OF TECHNOLOGY KANPUR   (India)

^b UNIVERSITY OF BARCELONA   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 55249091634     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic8011525     Document Type: Article

References (93)

1. (a) Clearfield, A. Progress in Inorganic Chemistry: Metal-Phosphonate Chemistry; Karlin, K. D., Ed.; John Wiley & Sons: New York, 1998; Vol. 47, pp 371-510; and references therein.
2. (b) Cao, G.; Hong, H.-G.; Mallouk, T. E. Acc. Chem. Res. 1992, 25, 420.
3. (c) Clearfield, A. Curr. Opin. Solid State Mater. Sci. 2002, 6, 495.
4. (d) Clearfield, A. Curr. Opin. Solid State Mater. Sci. 1996, 1, 268.
5. (e) Thompson, M. E. Chem. Mater. 1994, 6, 1168.
6. (f) Subbiah, A.; Pyle, D.; Rowland, A.; Huang, J.; Narayanan, R. A.; Thiyagarajan, P.; Zoń, J.; Clearfield, A. J. Am. Chem. Soc. 2005, 127, 10826.
7. (g) Song, S.-Y.; Ma, J.-F.; Yang, J.; Cao, M.-H.; Li, K.-C. Inorg. Chem. 2005, 44, 2140.
8. (h) Ouellette, W.; Yu, M. H.; O'Connor, C. J.; Zubieta, J. Inorg. Chem. 2006, 45, 7628.
9. (i) Ouellette, W.; Yu, M. H.; O'Connor, C. J.; Zubieta, J. Inorg. Chem. 2006, 45, 3224.
10. (j) Burkholder, E.; Golub, V.; O'Connor, C. J.; Zubieta, J. Inorg. Chem. 2004, 43, 7014.
11. (k) Yang, B.-P.; Mao, J.-G. Inorg. Chem. 2005, 44, 566.
12. (a) Wan, B.-Z.; Anthony, R. G.; Peng, G.-Z.; Clearfield, A. J. Catal. 1994, 19, 101.
13. (b) Deniaud, D.; Schollorn, B.; Mansury, J.; Rouxel, J.; Battion, P.; Bujoli, B. Chem. Mater. 1995, 7, 995.
14. (c) Hu, A.; Ngo, H.; Lin, W. J. Am. Chem. Soc. 2003, 125, 11490.
15. (d) Hu, A.; Yee, G. T.; Lin, W. J. Am. Chem. Soc. 2005, 127, 12486.
16. (e) Nonglaton, G.; Benitez, I. O.; Guisle, I.; Pipeler, M.; Leger, J.; Dubreuil, D.; Tellier, C.; Talham, D. R.; Bujoli, B. J. Am. Chem. Soc. 2004, 126, 1497.
17. (a) Clearfield, A. Inorganic Ion Exchange Materials; CRC Press: Boca Raton, FL, 1982.
18. (b) Alberti, G. In Comprehensive Supramolecular Chemistry; Alberti, G., Bein, T., Eds.: Pergamon: New York, 1996; Vol. 7. pp 151.
19. (C) Wang, J. D.; Clearfield, A.; Peng, G.-Z. Mater. Chem. Phys. 1993, 35, 208.
20. (d) Zang, B.; Clearfield, A. J. Am. Chem. Soc. 1997, 119, 2751.
21. (a) Fredoueil, F.; Massiot, D.; Janvier, P.; Gingl, F.; Bujoli-Doeuff, M.; Evian, M.; Clearfield, A.; Bujoli, B. Inorg. Chem. 1999, 38, 1831.
22. (b) Maeda, K.; Kiyozumi, Y.; Mizukami, F. J. Phys. Chem. B. 1997, 101, 4402.
23. (c) Yue, Q.; Yang, J.; Li, G.-H.; Li, G.-D.; Chen, J.-S. Inorg. Chem. 2006, 45, 4431.
24. (d) Gallagher, L. A.; Serron, S. A.; Wen, X.; Hornstein, B. J.; Dattelbaum, D. M.; Schoonover, J. R.; Meyer, T. J. Inorg. Chem. 2005, 44, 2089.
25. (e) Maeda, K. Microporous Mesoporous Mater. 2004, 73, 47.
26. (a) Ungashe, S. B.; Wilson, W. L.; Katz, H. E.; Scheller, G. R.; Putvinski, T. M. J. Am. Chem. Soc. 1992, 114, 8717.
27. (b) Sanchez-Moreno, M. J.; Fernandez-Botello, A.; Gomez-Coca, R. B.; Griesser, R.; Ochocki, J.; Kotynski, A.; Niclos-Gutierrez, J.; Moreno, V.; Sigel, H. Inorg. Chem. 2004, 43, 1311.
28. (c) Du, Z.-Y.; Xu, H.-B.; Mao, J.-G. Inorg. Chem. 2006, 45, 6424.
29. (a) Cabeza, A.; Aranda, M. A. G.; Bruque, S.; Poojary, D. M; Clearfield, A.; Sanz, J. Inorg. Chem. 1998, 37, 4168.
30. (b) Zhang, B.; Poojary, D. M.; Clearfield, A. Inorg. Chem. 1998, 37, 249.
31. (c) Ayyappan, P.; Evans, O. R.; Cui, Y.; Wheeler, K. A.; Lin, W. Inorg. Chem. 2002, 41, 4978.
32. (a) Chandrasekhar, V.; Kingsley, S. Angew. Chem., Int. Ed. 2000, 39, 2320.
33. (b) Chandrasekhar, V.; Kingsley, S.; Vij, A.; Lam, K. C.; Rheingold, A. L. Inorg. Chem. 2000, 39, 3238.
34. (c) Chandrasekhar, V.; Kingsley, S.; Hatigan, B.; Lam, M. K.; Rheingold, A. L. Inorg. Chem. 2002, 41, 1030.
35. (d) Chandrasekhar, V.; Nagarajan, L.; Gopal, K.; Baskar, V.; Kögerler, P. Dalton Trans. 2005, 3143.
36. (e) Chandrasekhar, V.; Sasikumar, P.; Boomishankar, R.; Anantharaman, G. Inorg. Chem. 2002, 41, 1030.
37. (a) Brechin, E. K.; Coxall, R. A.; Parkin, A.; Parsons, S.; Tasker, P. A.; Winpenny, R. E. P. Angew. Chem., Int. Ed. 2001, 40, 2700.
38. (b) Maheswaran, S.; Chastanet, G.; Teat, S. J.; Mallah, T.; Sessoli, R.; Wernsdorfer, W.; Winpenny, R. E. P. Angew. Chem., Int. Ed. 2005, 44, 5044.
39. (c) Tolis, E. I.; Helliwell, M.; Langley, S.; Raftery, J.; Winpenny, R. E. P. Angew. Chem., Int. Ed. 2003, 42, 3804.
40. (d) Langley, S. J.; Helliwell, M.; Sessoli, R.; Rosa, P.; Wernsdorfer, W.; Winpenny, R. E. P. Chem. Commun. 2005, 5029.
41. (e) Langley, S.; Helliwell, M.; Raftery, J.; Tolis, E. I.; Winpenny, R. E. P. Chem. Commun. 2004, 142.
42. (a) Walawalkar, M. G.; Roesky, H. W.; Murugavel, R. Acc. Chem. Res. 1999, 32, 117.
43. (b) Chakraborty, D.; Chandrasekhar, V.; Bhattacharjee, M.; Krätzner, R.; Roesky, H. W.; Noltemeyer, M.; Schmidt, H.-G. Inorg. Chem. 2000, 39, 23.
44. (c) Anantharaman, G.; Walawalkar, M. G.; Murugavel, R.; Gábor, B.; Regine, H.-I.; Baldus, M.; Angerstein, B.; Roesky, H. W. Angew. Chem., Int. Ed. 2003, 42, 4482.
45. (a) Konar, S.; Bhuvanesh, N.; Clearfield, A. J. Am. Chem. Soc. 2006, 128, 9604.
46. (b) Plutner, J.; Rohovec, J.; Kotek, J.; Žák, Z.; Lukeś, I. Inorg. Chim. Acta 2002, 335, 27.
47. (c) Liu, B.; Li, Y.-Z.; Zheng, L.-M. Inorg. Chem. 2005, 44, 6921.
48. (d) Cao, D.-K.; Li, Y.-Z.; Zheng, L.-M Inorg. Chem. 2005, 44, 2984.
49. (e) Yao, H.-C.; Li, Y.-Z.; Song, Y.; Ma, Y.-S.; Zheng, L.-M.; Xin, X.-Q. Inorg. Chem. 2006, 45, 59.
50. (f) Yao, H.-C.; Wang, J.-J.; Ma, Y.-S.; Waldmann, O.; Du, W.-X.; Song, Y.; Li, Y.-Z.; Zheng, L.-M.; Decurtins, S.; Xin, X.-Q. Chem. Commun. 2006, 1745.
51. (g) Kratochvil, J.; Necas, M.; Petricek, V.; Pinkas, J. Inorg. Chem. 2006, 45, 6562.
52. (h) Kontturi, M.; Laurilla, E.; Mattsson, R.; Peräniemi, S.; Vepsäläinen, J. J.; Ahlgrén, M. Inorg. Chem. 2005, 44, 2400.
53. (i) Mehring, M.; Guerrero, G.; Dahan, F.; Mutin, P. H.; Vioux, A. Inorg. Chem. 2000, 39, 3325.
54. (j) Otieno, T.; Mokry, L. M.; Bond, M. R.; Carrano, C. J.; Dean, N. S. Inorg. Chem. 1996, 35, 850.
55. (k) Clarke, R.; Latham, K.; Rix, C.; Hobday, M.; White, J. CrystEngComm 2004, 6, 42.
56. (l) Clarke, R.; Latham, K.; Rix, C.; Hobday, M.; White, J. CrystEngComm 2005, 7, 28.
57. (m) Yao, H.-C.; Li, Y.-Z.; Zheng, L.-M; Xin, X.-Q. Inorg. Chim. Acta 2005, 358, 2523.
58. (n) Yao, H.-C.; Li, Y.-Z.; Gao, S.; Song, Y.; Zheng, L.-M.; Xin, X.-Q. J. Solid State Chem. 2004, 177, 4557.
59. (o) Zhao, Q.-H.; Du, L.; Fang, R.-B. Acta Crystallogr. 2006, E62, m219.
60. (p) Yi, X.-Y.; Liu, B.; Jiménez-Aparico, R.; Urbanos, F. A.; Gao, G.; Xu, W.; Chen, J.-S.; Song, Y.; Zheng, L.-M. Inorg. Chem. 2005, 44, 4309.
61. (q) Fan, Y.-T.; Xue, D.-X.; Li, G.; Hou, H.-W.; Du, C.-X.; Lu, H.-J. J. Mol. Struct. 2004, 693, 217.
62. (r) Kontturi, M.; Peräniemi, S.; Vepsääinen, J. J.; Ahlgrén, M. Polyhedron 2005, 24, 305.
63. (s) Finn, R. C.; Zubieta, J. Inorg. Chim. Acta 2002, 332, 191.
64. Yang, Yu.; Walawalkar, M. G.; Pinkas, J.; Roesky, H. W.; Schmidt, H.-G. Angew. Chem., Int. Ed. 1998, 37, 96.
65. Baskar, V.; Shanmugam, M.; Sañudo, E. C.; Shanmugam, M.; Collison, D.; McInnes, E. J. L.; Wei, Q.; Winpenny, R. E. P. Chem. Commun. 2007, 37.
66. Anantharaman, G.; Walawalkar, M. G.; Murugavel, R.; Gábor, B.; Herbst-Irmer, R.; Baldus, M.; Angerstein, B.; Roesky, H. W. Angew. Chem., Int. Ed. 2003, 42, 4482.
67. Anantharaman, G.; Chandrasekhar, V.; Walawalkar, M. G.; Roesky, H. W.; Vidovic, D.; Magull, a J.; Noltemeyer, M. Dalton Trans. 2004, 1271.
68. Yang, Y.; Schmidt, H.-G.; Noltemeyer, M.; Pinkas, J.; Roesky, H. W. J. Chem. Soc. Dalton Trans. 1996, 3609.
69. Chandrasekhar, V.; Kingsley, S. Angew. Chem., Int. Ed. 2000, 39, 2320.
70. Chandrasekhar, V.; Kingsley, S.; Vij, A.; Lam, K. C.; Rheingold, A. L. Inorg. Chem. 2000, 39, 3238.
71. Chandrasekhar, V.; Kingsley, S.; Hatigan, B.; Lam, M. K.; Rheingold, A. L. Inorg. Chem. 2002, 41, 1030.
72. Chandrasekhar, V.; Sasikumar, P.; Boomishankar, R.; Anantharaman, G. Inorg. Chem. 2006, 45, 3344.
73. Chandrasekhar, V.; Nagarajan, L.; Gopal, K.; Baskar, V.; Kögerler, P. Dalton Trans. 2005, 3143.
74. Chandrasekhar, V.; Nagarajan, L.; Clerac, R.; Ghosh, S.; Senapati, T.; Verma, S. Inorg. Chem. 2008, 47, 5347.
75. Chandrasekhar, V.; Nagarajan, L.; Clerac, R.; Ghosh, S.; Verma, S. Inorg. Chem. 2008, 47, 1067.
76. Langley, S.; Helliwell, M.; Sessoli, R.; Teat, S. J.; Winpenny, R. E. P. Inorg. Chem. 2008, 47, 497.
77. Chandrasekhar, V.; Azhakar, R.; Senapati, T.; Thilagar, P.; Ghosh, S.; Verma, S.; Boomishankar, R.; Steiner, A.; Koegerler, P. Dalton Trans. 2008, 9, 1150.
78. Vogel's Textbook of Practical Organic Chemistry, 5th ed.; Longman: London, 1989.
79. (a) SMART & SAINT Software Reference manuals, Version 6.45; Bruker Analytical X-ray Systems, Inc.: Madison, WI, 2003.
80. (b) Sheldrick, G. M. SADABS a software for empirical absorption correction, Ver. 2.05; University of Goettingen: Goettingen, Germany, 2002.
81. (c) SHELXTL Reference Manual, Ver. 6.1; Bruker Analytical X-ray Systems, Inc.: Madison, WI, 2000.
82. (d) Sheldrick, G. M. SHELXTL, Ver. 6.12; Bruker AXS Inc.: Madison, WI, 2001.
83. (e) Sheldrick, G. M. SHELXL97, Program for Crystal Structure Refinement; University of Geottingen: Goettingen, Germany, 1997.
84. (f) Bradenburg, K. Diamond, Ver. 3.1eM; Crystal Impact GbR: Bonn, Germany, 2005.
85. Coxall, R. A.; Harris, S. G.; Henderson, S.; Parsons, S.; Taskar, R. A.; Winpenny, R. E. P. J. Chem. Soc., Dalton Trans. 2000, 14, 2349.
86. (a) Fernandez-Botello, A.; Escure, A.; Solans, X.; Font-Bardia, M.; Holy, A.; Sigel, H.; Moreno, V. Eur. J. Inorg. Chem. 2007, 1867.
87. (b) Itoh, M.; Nakazawa, J.; Maeda, K.; Kano, K.; Mizutani, T.; Kodera, M. Inorg. Chem. 2005, 44, 691.
88. (c) Liu, X.; McLaughlin, A. C.; de Miranda, M. P.; McInnes, E. J. L.; Kilner, C. A.; Halcrow, M. A. Chem. Commun. 2002, 2978.
89. (d) Mezei, G.; Baran, P.; Raptis, R. G. Angew. Chem., Int. Ed. 2004, 43, 574.
90. (e) Mohamed, A. A.; Burini, A.; Galassi, R.; Paglialunga, D.; Galan-Mascaros, J.-R.; Dunbar, K. R.; Fackler, J. P., Jr. Inorg. Chem. 2007, 46, 2348.
91. (f) Sakai, K.; Yamada, Y.; Tsubomura, T.; Yabuki, M.; Yamaguchi, M. Inorg. Chem. 1996, 542.
92. Borrás-Almenar, J. J.; Clemente-Juan, J. M.; Coronado, E.; Tsukerblat, B. S. (Magpack Software) J. Comp. Chem. 2001, 2, 2985.
93. Kahn, O. Molecular Magnetism; VCH Publishers: New York, 1993; p 26.