Liquid chromatography-mass spectrometry-based quantification of steroidal glycoalkaloids from Solanum xanthocarpum and effect of different extraction methods on their content

Journal of Chromatography A

Volumn 1208, Issue 1-2, 2008, Pages 141-146

  Paul, Atish T ^a   Vir, Sanjay ^a   Bhutani, K K ^a  

^a NATIONAL INSTITUTE OF PHARMACEUTICAL EDUCATION AND RESEARCH NIPER   (India)

Author keywords

Fingerprint analysis; LC MS; Method validation; PLE; S. xanthocarpum; SGAs

Indexed keywords

ACETONITRILE; ACIDS; BODY FLUIDS; CELL CULTURE; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; COLUMNS (STRUCTURAL); CUSTOMER SATISFACTION; FORMIC ACID; GRADIENT METHODS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; MASS SPECTROMETERS; MASS SPECTROMETRY; ORGANIC ACIDS; QUALITY ASSURANCE; QUALITY CONTROL; QUALITY FUNCTION DEPLOYMENT; SENSITIVITY ANALYSIS; SEPARATION; SOLVENT EXTRACTION; SPECTROMETERS; SPECTROMETRY; SPECTRUM ANALYSIS; STANDARDIZATION; TOTAL QUALITY MANAGEMENT;

FINGERPRINT ANALYSIS; LC-MS; METHOD VALIDATION; PLE; S. XANTHOCARPUM; SGAS;

EXTRACTION;

2 PROPANOL; ACETONITRILE; ANTIPYRETIC AGENT; BETA 2 SOLAMARGINE; FORMIC ACID; PLANT EXTRACT; SAPONIN DERIVATIVE; SOLAMARGINE; SOLANACARPINE; SOLANUM XANTHOCARPUM EXTRACT; SOLASONINE; STEROIDAL GLYCOALKALOID; UNCLASSIFIED DRUG; WATER;

ARTICLE; CALIBRATION; DRUG ACTIVITY; DRUG STRUCTURE; ELUTION; FLOW RATE; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; MEDICINAL PLANT; PRIORITY JOURNAL; QUALITY CONTROL; SENSITIVITY ANALYSIS; SOLANUM XANTHOCARPUM; SOXHLET EXTRACTION;

ANALYTIC SAMPLE PREPARATION METHODS; CHROMATOGRAPHY, LIQUID; MASS SPECTROMETRY; SENSITIVITY AND SPECIFICITY; SOLANACEOUS ALKALOIDS; SOLANUM;

SOLANUM XANTHOCARPUM;

EID: 53249098388     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2008.08.089     Document Type: Article

References (44)

1. Vaananen T., Kuronen P., and Pehu E. J. Chromatogr. A 869 (2000) 301
2. Oleszek W. J. Chromatogr. A 967 (2002) 147
3. Li S.L., Lin G., Chan S.W., and Li P. J. Chromatogr. A 909 (2001) 207
4. Li P., Zeng L.J., Li S.L., and Lin G. Phytochem. Anal. 13 (2002) 158
5. Zhou J.L., Li P., Li H.J., Jiang Y., Ren M.T., and Liu Y. J. Chromatogr. A 1177 (2008) 126
6. Oleszek W., and Bialy Z. J. Chromatogr. A 1112 (2006) 78
7. Cui M., Song F., Zhou Y., Liu Z., and Liu S. Rapid Commun. Mass Spectrom. 14 (2000) 1280
8. Kite G.C., Howes M.J.R., Leon C.J., and Simmonds M.S.J. Rapid Commun. Mass Spectrom. 17 (2003) 238
9. Fuzzati N., Pace R., Papeo G., and Peterlongo F. J. Chromatogr. A 777 (1997) 233
10. Zhou Y., Wang M.K., Liao X., Zhu X.M., Peng S.L., and Ding L.S. Chin. J. Anal. Chem. 32 (2004) 74
11. Wang M.K., Liang C.-P., Wu Q.-L., Simon J.E., and Ho C.-T. In: Wang M., Sang, Hwang L.S., and Ho C.-T. (Eds). Herbs: Challenges in Chemistry Biology (2006), American Chemical Society, Washington, DC 39
12. De Combarieu E., Fuzzati N., Lovati M., and Mercalli E. Fitoterapia 74 (2003) 583
13. Jensen P.H., Juhler R.K., Nielsen N.J., Hansen T.H., Strobel B.W., Jacobsen O.S., Nielsen J., and Hansen H.C.B. J. Chromatogr. A 1182 (2008) 65
14. Zywicki B., Catchpole G., Draper J., and Fiehn O. Anal. Biochem. 336 (2005) 178
15. Matsuda F., Morino K., Miyazawa H., Miyashita M., and Miyagawa H. Phytochem. Anal. 15 (2004) 121
16. Vaananen T., Ikonen T., Rokka V.M., Kuronen P., Serimaa R., and Ollilainen V. J. Agric. Food Chem. 53 (2005) 5313
17. Anonymous, The Wealth of India-Raw materials, vol. IX: Rh-So, CSIR, New Delhi, 1989, p. 393.
18. Anonymous, Indian Herbal Pharmacopoeia, vol. I, Indian Drug Manufacturers' Association, 355 Mumbai and Regional Research Laboratory, Jammu Tawi, 1998, p. 139.
19. Kiritikar K.R., and Basu B.D. Indian Medicinal Plants. 2nd ed. vol. III (1994), Bishen Singh, Mahendra Pal Singh, Dehradun p. 1759
20. Jain S.P., and Puri H.S. J. Ethnopharmacol. 12 (1984) 213
21. Gupta S.S., Rai M., and Gupta N.K. Curr. Sci. 36 (1967) 42
22. Dhar M.L., Dhar M.M., Dhawan B.N., Mehrotra B.N., and Ray C. Ind. J. Exp. Biol. 6 (1968) 232
23. Smit H.F., Woerdenbag H.J., Singh R.H., Meulenbeld G.J., Labadie R.P., and Zwaving J.H. J. Ethnopharmacol. 47 (1995) 75
24. Gupta M.P., and Dutt S. J. Ind. Chem. Soc. 15 (1938) 95
25. Saived I.Z. Proc. Ind. Acad. Sci. Series A4 (1963) 255
26. Siddiqui S., Faizi S., and Shaheen B. J. Chem. Soc. Pak. 5 (1983) 99
27. Tupkari S.V., Saoji A.N., and Deshmukh V.K. Planta Med. 22 (1972) 184
28. Sato Y., and Latham J.R. J. Am. Chem. Soc. 75 (1953) 6067
29. Kusano G., Beisler J., and Sato Y. Phytochemistry 12 (1973) 397
30. Abreu P., Relva A., Matthew S., Gomes Z., and Morais Z. Food Control 18 (2007) 40
31. Verbist J.F., and Monnet R. Plant Med. Phytother. 8 (1974) 269
32. Trivedi P.D., and Pundarikakshudu K. Chromatographia 65 (2007) 239
33. Usubillaga A., Aziz I., Tettamanzi M.C., Waibel R., and Achenbach H. Phytochemistry 44 (1997) 537
34. Dictionary of Natural Products 1982-2003, Chapman & Hall/CRC, London, 2003.
35. Eldridge A.C., and Hockridge M.E. J. Agric. Food Chem. 31 (1983) 1218
36. Kuronen P., Vaananen T., and Pehu E. J. Chromatogr. A 863 (1999) 25
37. Bushway R.J., Perkins L.B., Paradis L.R., and Vanderplan S. J. Agric. Food Chem. 42 (1994) 2824
38. Bushway R.J., Bureau J.L., and King J.L. J. Agric. Food Chem. 34 (1986) 277
39. Keukens E.A.J., Hop M.E.C.M., and Jongen W.M.F. J. Agric. Food Chem. 42 (1994) 2475
40. Saito K., Horie M., Hoshing Y., and Nose N. J. Chromatogr. 508 (1990) 141
41. International Conference on Harmonization of Technical Requirements for the Registration of Pharmaceuticals for Human Use (ICH), Guideline Q2BValidation of Analytical Procedures: Methodology, ICH Secretariat, c/o IFPMA, Geneva, 1996, p. 1.
42. Magrini E., Giulietti A.M., Wilson E., and Cascone O. Biotechnol. Tech. 3 (1989) 185
43. Jonker H.H., Koops A.J., and Hoogendoorn J.C. Potato Res. 35 (1992) 451
44. Friedman M., Roitman J.N., and Kozukue N. J. Agric. Food Chem. 51 (2003) 2964