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4), concentrated in vacuo, and purified by silical gel column chromatography (hexane/ethyl acetate, 4/1, v/v) to give 6 as a white solid in 50% yield.
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4), concentrated in vacuo, and purified by silical gel column chromatography (hexane/ethyl acetate, 4/1, v/v) to give 6 as a white solid in 50% yield.
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