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47049092579
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2O)}
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60 (706.45): C 47.60%; H 8.56%; N 3.96%; S 9.08%. Found C 47.46%; H 8.79%; N 3.91%; S 8.84. Yield 46%.
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27
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47049129758
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1
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-3). Two of tBu residues are disordered over two positions with occupancy factors 70-30 (C17, C18, C19, C20) and 78-22 (C22, C23, C24). Soft restraints SIMU were used on the thermal ellipsoids of the disordered atoms to prevent them from going "non-positive definite". DFIX restraint (1.52 Å with standard deviation of 0.01) was also applied to the length of C21-C23A bond.
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30
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47049097137
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-1 FT-IR spectra of 1, 2 and 3 are available as supplementary materials.
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-1 FT-IR spectra of 1, 2 and 3 are available as supplementary materials.
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