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note
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As very often observed for complexes of this kind, inclusion solvent is observed despite thorough pumping, preventing good elemental analysis.
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49
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84942435207
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The contribution of the disordered solvents to the calculated structure factors was estimated following the BYPASS algorithm, implemented as the SQUEEZE option in PLATON. A new data set, free of solvent contribution, was then used in the final refinement. See:
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The contribution of the disordered solvents to the calculated structure factors was estimated following the BYPASS algorithm, implemented as the SQUEEZE option in PLATON. A new data set, free of solvent contribution, was then used in the final refinement. See:. Sluis P.v.d., and Spek A.L. Acta Cryst. A 46 (1990) 194-201
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