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Polymer 2 was found in this case to have an absorption maximum at 505 nm, in contrast to 494 nm in Barton's studies. This slight discrepancy can likely be ascribed to different solvents.
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(a) For similar observations in silole cross couplings, see: Ohshita, J.; Mimura, N.; Arase, H.; Nodono, M.; Kunai, A.; Komaguchi, K.; Shiotani, M.; Ishikawa, M. Macromolecules 1998, 31, 7985-7987.
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4143089368
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Reference 15
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(b) Reference 15.
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52
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4143075914
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note
-
2-Ethynyl-1,1-dimethyl-3,4-diphenyl-5-(phenylethynyl)silole and 2-chloro-5-ethynyl-1,1-dimethyl-3,4-diphenylsilole were also found to be unstable under the cross-coupling reaction conditions and decomposed upon prolonged storage.
-
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53
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4143111391
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note
-
This is not a general limitation: solubility can be modulated by the use of larger 1,1-diatkyl siloles.
-
-
-
-
55
-
-
4143073721
-
-
note
-
Compounds exactly analogous to 6 have been prepared from 2,5-dibromosiloles; see refs 11b and 15.
-
-
-
-
56
-
-
4143087161
-
-
note
-
These results will be reported elsewhere.
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57
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0028405746
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Pearson, D. L.; Schumm, J. S.; Tour, J. M. Macromolecules 1994, 27, 2348-2350.
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4143135436
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note
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For example, pentamer 10 is counted as an 11-mer.
-
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61
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0001605471
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and references therein
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4143114679
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-
note
-
F was determined with reference to fluorescein.
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-
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