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34547655485
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note
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2 (30%) from Merck was used as received. The peroxide content varied from 33% to 40% as determined by titration.
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note
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Side-products are rearrangement products of the corresponding epoxide.
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note
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Most of the substrates and epoxides for GC-FID calibration are commercially available. The others were synthesized according to literature methods and determined by NMR and GC-MS. In addition, authentic samples of the commercial products were analyzed by GC-MS and GC-FID.
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