Quantitation and validation of fluoroquinolones in eggs using liquid chromatography/tandem mass spectrometry

Journal of AOAC International

Volumn 90, Issue 2, 2007, Pages 613-625

  Durden, David A ^a   MacPherson, Tanya ^a  

^a CANADIAN FOOD INSPECTION AGENCY   (Canada)

Author keywords

[No Author keywords available]

Indexed keywords

ACETONITRILE; BIRDS; CHEMICAL ANALYSIS; FOOD PRODUCTS; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY;

ENROFLOXACIN; FLUOROQUINOLONES; NORFLOXACIN; TANDEM MASS SPECTROMETRY;

ANTIBIOTICS;

ANIMALIA; AVES;

ANTIINFECTIVE AGENT; DRUG RESIDUE; METHANOL; PHOSPHATE; QUINOLONE DERIVATIVE;

ANIMAL; ARTICLE; CALIBRATION; CHEMICAL MODEL; CHEMISTRY; EGG; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; METHODOLOGY; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY;

ANIMALS; ANTI-BACTERIAL AGENTS; CALIBRATION; CHEMISTRY, ANALYTICAL; CHROMATOGRAPHY, LIQUID; DRUG RESIDUES; EGGS; FLUOROQUINOLONES; MASS SPECTROMETRY; METHANOL; MODELS, CHEMICAL; PHOSPHATES; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY;

EID: 34447623576     PISSN: 10603271     EISSN: None     Source Type: Journal    
DOI: 10.1093/jaoac/90.2.613     Document Type: Article

References (41)

1. U.S. Food and Drug Administration (2006) Title 21, Food and Drug Administration U.S. Department of Health and Human Services, Animal Drugs, Feeds, and Related Products: Part 556 Tolerances for Residues of New Animal Drugs in Food, http://www.accessdata.fda.gov/scripts/cdrh/cfdocs/cfcfr/ CFRSearch.cfm?CFRPart=556
2. EMEA (2006) European Medicines Agency, Veterinary Medicines, http://www.emea.europa.eu/ index/indexv1.htm
3. Health Canada (2002) Uses of Antimicrobials in Food Animals in Canada: Impact on Resistance and Human Health: Antimicrobials registered for use in animals and humans in Canada, http://www.hc-sc.gc.ca/dhp-mps/pubs/vet/amr- ram_final_report-rapport_06-27_table_9_e.html
4. Health Canada (2005) Administrative Maximum Residue Limits (AMRLS) and Maximum Residue Limits (MRLS) set by Canada, http://www.hc-sc.gc.ca/dhp-mps/vet/ mrl-lmr/mrl-lmr_versus_new-nouveau_e.html
5. Martinez, M., McDermott, P., & Walker, R. (2006) Vet. J. 172, 10-28
6. Gorla, N., Chiostri, E., Ugnia, L., Weyers, A., Giacomelli, N., Davicino, R., & Ovando, H.G. (1997) Int. J. Antimicrob. Agents 8, 253-256
7. Maxwell, R.J., Cohen, E., & Donaoghue, D.J. (1999) J. Agric. Food Chem. 47, 1563-1567
8. Donoghue, D.J., & Schneider, M.J. (2003) J. AOAC Int. 86, 669-674
9. Livermore, D.M., James, D., Reacher, M., Graham, C., Nichols, T., Stephens, P., Johnson, A.P., & George, R.C. (2002) Emerg. Infect. Dis. 8, 473-478
10. Woodford, N. (2005) Clin. Microbiol. Infect. 11 (Suppl. 3), 2-21
11. McDermott, P.F., Zhao, S., Wagner, D.D., Simjee, S., Walker, R.D., & White, D.G. (2002) Anim. Biotechnol. 13, 71-84
12. Cox, L.A., Jr, & Popken, D.A. (2006) Risk Anal. 26, 135-146
13. Aarestrup, F.M., Seyfarth, A.M., Emborg, H.D., Pedersen, K., Hendriksen, R.S., & Bager, F. (2001) Antimicrob. Agents Chemother. 45, 2054-2059
14. U.S. Food and Drug Administration (2005) Fed. Reg. 70, Docket No. 2000N-1571, August 1
15. U.S. Food and Drug Administration (2001) Fed. Reg. 66, Docket No. 01N-0170, April 30
16. Schneider, M.J., & Donoghue, D.J. (2000)J. AOAC Int. 83, 1306-1312
17. Rose, M.D., Bygrave, J., & Stubbings, G.W. (1998) Analyst 123, 2789-2796
18. Verdon, E., Couedor, P., Roudaut, B., & Sanders, P. (2005) J. AOAC Int. 88, 1179-1192
19. Turnipseed, S.B., Walker, C.C., Roybal, J.E., Pfenning, A.P., & Hurlbut, J.A. (1998) J. AOAC Int. 81, 554-562
20. Volmer, D.A., Mansoori, B., & Locke, S.J. (1997) Anal. Chem. 69, 4143-4155
21. Schneider, R.P., Ericson, J.F., Lynch, M.J., & Fouda, H.G. (1993) Biol. Mass Spectrom. 22, 595-599
22. Engler, M., Rusing, G., Sorgel, F., & Holzgrabe, U. (1998) Antimicrob. Agents Chemother. 42, 1151-1159
23. Toussaint, B., Bordin, G., Janosi, A., & Rodriguez, A.R. (2002) J. Chromatogr. A 976, 195-206
24. Schneider, M., & Donoghue, D. (2002) J. Chromatogr. B Anal. Technol. Biomed. Life Sci. 780, 83-92
25. Toussaint, B., Chedin, M., Bordin, G., & Rodriguez, A.R. (2005) J. Chromatogr. A 1088, 32-39
26. Almeida, A.M., Castel-Branco, M.M., & Falcao, A.C. (2002) J. Chromatogr. B 774, 215-222
27. Plackett, R.L., & Burman, J.P. (1946) Biometrika 33, 305-325
28. Vander Heyden, Y., Nijhuis, A., Smeyers-Verbeke, J., Vandeginste, B.G., & Massart, D.L. (2001) J. Pharm. Biomed. Anal. 24, 723-753
29. Lolo, M., Pedreira, S., Fente, C., Vazquez, B.I., Franco, C.M., & Cepeda, A. (2005) J. Agric. Food Chem. 53, 2849-2852
30. McLafferty, F.W., & Turacek, F. (1993) Interpretation of Mass Spectra, University Science Books, Mill Valley, CA
31. Ballesteros, O., Toro, I., Sanz Nebot, V., Navalon, A., Vilchez, J.L., & Barbosa, J. (2003) J. Chromatogr. B 798, 137-144
32. Roybal, J.E., Pfenning, A.P., Turnipseed, S.B., Walker, C.C., & Hurlbut, J.A. (1997) J. AOAC Int. 80, 982-987
33. U.S. Department of Agriculture (2006) National Nutrient Database for Standard Reference, http://www.nal.usda.gov/fnic/foodcomp/search/
34. Jenkins, K.M., & Young, M.S. (2003) Validation of a Method for Determination of Fluoroquinolone Antibiotics in Bovine Tissue by LC/MS or LC-fluorescence, 226th ACS National Meeting, New York, NY, http://www.waters.com/WATERSDIVISION/pdfs/WA31770.pdf
35. Miller, J.N., & Miller, J.C. (2000) Statistics and Chemometrics for Analytical Chemistry, Prentice Hall, Harlow, UK
36. European Commission Decision 2002/657/EC (2002) Off. J. Eur. Commun. L221, 228-236
37. ISO 11843-2 (2000) Capability of Detection-Part 2: Methodology in the Linear Calibration Case, International Organization for Standardization, Geneva, Switzerland
38. Matuszewski, B.K., Constanzer, M.L., & Chavez-Eng, C.M. (1998) Anal. Chem. 70, 882-889
39. Barwick, V.J., & Ellison, S.L.R. (2000) Development and Harmonization of Measurement Uncertainty Principles Part (d): Protocol for Uncertainty Evaluation from Validation Data, in VAM Technical Report No. LGC/VAM/1998/088
40. Youden, W.J. (1975) in Statistical Manual of the Association of Official Analytical Chemists, W.J. Youden & E.H. Steiner (Eds), Association of Official Analytical Chemists, Arlington, VA, pp 1-63
41. Waters, R.B., & Dovletoglou, A. (2003) J. Liq. Chromatogr. Rel. Technol. 26, 2975-2985