Determination of sarafloxacin residues in fortified and incurred eggs using on-line microdialysis and HPLC/programmable fluorescence detection

Journal of Agricultural and Food Chemistry

Volumn 47, Issue 4, 1999, Pages 1563-1567

  Maxwell, Robert J ^a   Cohen, Evjatar ^a   Donoghue, Dan J ^b  

^a EASTERN REGIONAL RESEARCH CENTER   (United States)

^b CENTER FOR DRUG EVALUATION AND RESEARCH   (United States)

Author keywords

ASTED; Chicken; Eggs; Fluorescence; HPLC; On line microdialysis; Sarafloxacin

Indexed keywords

ANTIBIOTIC AGENT; CIPROFLOXACIN; DRUG DERIVATIVE; DRUG RESIDUE; NORDIFLOXACIN; QUINOLINE DERIVED ANTIINFECTIVE AGENT;

ANALYTIC METHOD; ANIMAL; ANIMAL EXPERIMENT; ANTIBIOTIC THERAPY; ARTICLE; AUTOMATION; CHICKEN; CONTROLLED STUDY; DRUG DETERMINATION; EGG; EGG LAYING; FEMALE; FLUORESCENCE; FOOD CONTAMINATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; INFECTION CONTROL; INTRAMUSCULAR DRUG ADMINISTRATION; METHODOLOGY; MICRODIALYSIS; NONHUMAN;

ANIMALIA; GALLUS GALLUS;

EID: 0032936284     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf980986k     Document Type: Article

References (22)

1. Acar, J. F.; Francoual, S. The clinical problems of bacterial resistance to the new quinolones. J. Antimicrob. Chemother. 1990, 26 (Suppl. B), 207-213.
2. Acar, J. F.; Goldstein, F. W. Trends in bacterial resistance to fluoroquinolones. Clin. Infect. Dis. 1997, 24 (Suppl. 1), S67-S73.
3. Acar, J. F.; O'Brien, T. F.; Goldstein, F. W.; Jones, R. N. The epidemiology of bacterial resistance to quinolones. Drugs 1993, 45 (Suppl. 3), 24-28.
4. Aerts, M. M. L.; Beek, W. M. J.; Brinkman, U. A. Th. Monitoring of veterinary drug residues by a combination of continuous flow techniques and column-switching HPLC. J. Chromatogr. 1988, 435, 97-112.
5. Aerts, R. M. L.; Egberink, I. M.; Kan, C. A.; Keukens, H. J.; Beek, W. M. J. Liquid chromatographic multicomponent method for determination of residues of ipronidazole, ronidazole, and dimetridazole and some relevant metabolites in eggs, plasma, and feces and its use in depletion studies in laying hens. J. Assoc. Off. Anal. Chem. 1991, 74, 46-55.
6. Aerts, M. M. L.; Hogenboom, A. C.; Brinkman, U. A. Th. Analytical strategies for the screening of veterinary drugs and their residues in edible products. J. Chromatogr. B 1995, 667, 1-40.
7. Andresen, A.; Rasmussen, K. Automated on-line dialysis and column-switching HPLC determination of flumequine and oxolinic acid in fish liver. J. Liq. Chromatogr. 1990, 13, 4051-4065.
8. Buick, A. R.; Fook Sheung, C. T. C. Determination of 1-(β-D-arabinofuranosyl)-5-(1-propynyl)-uracil and a metabolite, 5-propynyluracil, in plasma using ASTED (automated trace enrichment of dialysates) combined, on-line, with high-performance liquid chromatography. J. Chromatogr. Biomed. Appl. 1993, 617, 65-70.
9. Cohen, E.; Maxwell, R. J.; Donoghue, D. J. Automated multiresidue isolation of fluoroquinolone antimicrobials from fortified and incurred chicken liver using on-line microdialysis and HPLC with programmable fluorescence detection. J. Chromatogr. B 1999, 724, 137-145.
10. Donoghue, D. J.; Herman, H.; Henderson, M.; McDonald, M.; Gaines, S.; Donoghue, A. M. Modeling drug residue uptake by eggs: yolks contain ampicillin residues even after drug withdrawal and nondetectability in the plasma. Poult. Sci. 1897, 76, 458-462.
11. Endtz, H. P.; Ruijs, G. J.; Van Klingeren, B.; Jansen, W. H.; van der Reyden, T.; Mouten, R. P. Quinolone resistance in Campylobacter isolated from man and poultry following the introduction of fluoroquinolones in veterinary medicine. J. Antimicrob. Chemother. 1991, 27, 199-208.
12. Eng, G. Y.; Maxwell, R. J.; Cohen, E.; Piotrowski, E. G.; Fiddler, W. Determination of flumequine and oxolinic acid in fortified chicken tissue using on-line dialysis and HPLC with fluorescence detection. J. Chromatogr. A 1998, 799, 349-354.
13. Federal Register. Rules and regulations part 522-Implantation of injectable dosage from new drugs. Sec. 522.2095 sarafloxacin solution for injection. Fed. Regist. 1995, 60, 225.
14. Federal Register. Rules and Regulations Part 540. Fed. Regist. 1997, 62 (99), 27944.
15. Gorla, N.; Chiostri, E.; Ugnia, L.; Weyers, A.; Giacomelli, G.; Davicino, R.; Ovando, H. G. HPLC residues of enrofloxacin and ciprofloxacin in eggs of laying hens. Int. J. Antimicrob. Agents 1997, 8, 253-256.
16. Hormazabal, V.; Rogstad, A.; Steffenak, I.; Yndestad, M. Rapid assay for monitoring residues of enrofloxacin and sarafloxacin in fish tissues by HPLC. J. Liq. Chromatogr. 1991, 14, 1605-1614.
17. Horwitz, W.; Kamps, L. R.; Boyer, K. W. Quality assurance in the analysis of foods for trace constituents. J. Assoc. Off. Anal. Chem. 1980, 63, 1344-1354.
18. Maxwell, R. J.; Cohen, E. Comparison of programmable versus single wavelength fluorescence detection of three fluoroquinolone antibacterials isolated from fortified chicken liver using coupled on-line microdialysis and HPLC. J. High Resolut. Chromatogr. 1998, 21, 241-244.
19. Schwaiger, I.; Schuch, R. HPLC determination of residues of enrofloxacin and its primary metabolite ciprofloxacin in eggs and poultry tissue. Ernaehrung 1997, 21, 318-320.
20. Thanh, H. H.; Andresen, A. T.; Agasøster T.; Rasmussen, K. E. Automated column-switching HPLC determination of flumequine and oxolinic acid in extracts from fish. J. Chromatogr. 1990, 532, 363-373.
21. Turnell D. C.; Cooper, J. D. H. Automated sequential process for preparing samples for analysis by HPLC. J. Chromatogr. 1987, 395, 613-321.
22. Walker, C. C.; Storey, J. M.; Roybal, J. E.; Pfenning, A. P.; Plakas, S. M.; Turnipseed, S. B. Simultaneous determination of ciprofloxacin, enrofloxacin, sarafloxacin and difloxacin residues in catfish muscle by liquid chromatography with fluorescence detection. Lab. Inf. Bul., HHS, PHS, FDA 1996, 12d, 8.