Validation according to European Commission Decision 2002/657/EC of a confirmatory method for aflatoxin M1 in milk based on immunoaffinity columns and high performance liquid chromatography with fluorescence detection

Analytica Chimica Acta

Volumn 594, Issue 2, 2007, Pages 257-264

  Muscarella, Marilena ^a   Magro, Sonia Lo ^a   Palermo, Carmen ^b   Centonze, Diego ^b  

^a ISTITUTO ZOOPROFILATTICO SPERIMENTALE DELLA PUGLIA E DELLA BASILICATA   (Italy)

^b UNIVERSITY OF FOGGIA   (Italy)

Author keywords

2002 657 EC; Aflatoxin M1; Fluorescence detection; High performance liquid chromatography; Milk; Validation

Indexed keywords

FLUORESCENCE; HEAT TREATMENT; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

DETECTION CAPABILITY; FLUORIMETRIC DETECTION; LIMIT OF DETECTION (LOD); LIMIT OF QUANTITATION (LOQ);

AFLATOXINS;

AFLATOXIN M1;

ACCURACY; ANALYTIC METHOD; ARTICLE; FLUORESCENCE ANALYSIS; HEAT TREATMENT; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IMMUNOAFFINITY CHROMATOGRAPHY; LABORATORY TEST; MILK; PRIORITY JOURNAL; REPRODUCIBILITY; SCREENING TEST; STORAGE; TOXIN ANALYSIS; VALIDATION STUDY;

AFLATOXIN M1; ANIMALS; CARCINOGENS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; FLUORESCENCE; FLUOROMETRY; FOOD CONTAMINATION; MILK;

CAPRA HIRCUS; OVIS ARIES;

EID: 34250616735     PISSN: 00032670     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.aca.2007.05.029     Document Type: Article

References (45)

1. Sweeney M.J., and Dobson A.D.W. Int. J. Food Microbiol. 43 (1998) 141-158
2. Hussein H.S., and Brasel J.M. Toxicology 167 (2001) 101-134
3. Peraica M., Radic B., Lucic A., and Pavlovic M. World Health Organ. 77 (1999) 754-756
4. In: Eaton D.L., and Groopman J.D. (Eds). The Toxicology of Aflatoxins (1994), Academic Press, New York 383-426
5. International Agency for Research on Cancer (IARC). IARC Monographs on the Evaluation of Carcinogenic Risks to Humans 56 (1993), Lyon pp. 245-362
6. van Egmond H.P. Mycotoxins in Dairy Products (1989), Elsevier Applied Science, London, New York pp. 1-54
7. International Agency for Research on Cancer (IARC). IARC Monographs on the Evaluation of Carcinogenic Risks to Humans 56 (2002), Lyon pp.171-176
8. Stoloff L. J. Food Prot. 43 (1980) 226-230
9. European Parliament and Council. Directive 96/23/EC of 23 May 1996. Off. J. European Union L125 (1996) 10-16
10. European Commission. Regulation (EC) No. 466/2001 of 8 March 2001. Off. J. European Union L77 (2001) 1-13
11. European Commission. Regulation (EC) No. 683/2004 of 13 April 2004 amending Regulation (EC) No. 466/2001. Off. J. European Union L106 (2004) 3-5
12. Thirumala-Devi K., Mayo M.A., Hall A.J., Craufurd P.Q., Wheeler T.R., Waliyar F., Subrahmanyam A., and Reddy D.V.R. J. Agric. Food Chem. 50 (2002) 933-937
13. Magliulo M., Mirasoli M., Simoni P., Lelli R., Portanti O., and Roda A. J. Agric. Food Chem. 53 (2005) 3300-3305
14. Stroka J., and Anklam E. Trends Anal. Chem. 21 (2002) 90-95
15. Micheli L., Greco R., Badea M., Moscone D., and Palleschi G. Biosens. Bioelectron. 21 4 (2005) 588-596
16. Badea M., Micheli L., Messia M.C., Cardigliota T., Marconi E., Mottram T., Valesco-Garcia M., Moscone D., and Palleschi G. Anal. Chim. Acta 520 (2004) 141-148
17. Blesa J., Soriano J.M., Molto J.C., Marin R., and Manes J. J. Chromatogr. A 1011 (2003) 49-54
18. Tavčar-Kalcher G., Vrtač K., Pestevšek U., and Vengušt A. Food Control 18 (2007) 333-337
19. Chan D., MacDonald S.J., Boughtflower V., and Brereton P. J. Chromatogr. A 1059 (2004) 13-16
20. Abbas H.K., Williams W.P., Windham G.L., Pringle H.C., Xie W., and Shier W.T. J. Agric. Food Chem. 50 (2002) 5246-5254
21. Cavaliere C., Foglia P., Pastorini E., Samperi R., and Laganà A. J. Chromatogr. A 1101 1/2 (2006) 69-78
22. Gilbert J., and Anklam E. Trends Anal. Chem. 21 (2002) 468-486
23. Simon P., Delsaut P., Lafntaine M., Morele Y., and Nicot T. J. Chromatogr. B 712 (1998) 95-104
24. Chiavaro E., Dall'Asta C., Galaverna G., Biancardi A., Gambarelli E., Dossena A., and Marchelli R. J. Chromatogr. A 937 (2001) 31-40
25. Gilbert J., and Anklam E. Trends Anal. Chem. 21 6/7 (2002) 468-486
26. Gallo P., Salzillo A., Rossini C., Urbani V., and Serpe L. Ital. J. Food Sci. 3 18 (2006) 251-259
27. Manetta A.C., Di Giuseppe L., Giammarco M., Fusaro I., Simonella A., Gramenzi A., and Formigoni A. J. Chromatogr. A 1083 (2005) 219-222
28. European Commission. Regulation (EC) No. 401/2006 of 23 February 2006. Off. J. European Union L70 (2006) 12-34
29. European Commission. Decision 2002/657/EC of 12 August 2002. Off. J. European Union L221 (2002) 8-36
30. European Commission. Regulation (EC) No. 882/2004 of 29 April 2004. Off. J. European Union L165 (2004) 1-141
31. UNI CEI EN ISO/IEC 17025 (2000).
32. Association of Official Analytical Chemists (AOAC). EDN sixteenth ed. Official Methods of Analysis of AOAC II n.971.22 (1997), AOAC, Gaithersburg
33. Mortimer D.N., Gilbert J., and Shepherd M.J. J. Chromatogr. 407 (1987) 393-398
34. ISTISAN Report 96/34, ISSN 1123-3177 (1996) 218-219.
35. Pecorelli I., Bibi R., Fioroni L., and Galarini R. J. Chromatogr. A 1032 (2004) 23-29
36. Scortichini G., Annunziata L., Haouet M.N., Benedetti F., Krusteva I., and Galarini R. Anal. Chim. Acta 535 (2005) 43-48
37. Miller E.J.C., and Miller J.N. Statistics for Analytical Chemistry. third ed. (1993), Ellis Horwood TR Prentice-Hall, West Sussex, UK pp. 115-117
38. Youden W.J., and Steiner E.H. Statistical Manual of AOAC (1975), Association of Official Analytical Chemists, Gaithersburg pp. 33-35
39. Van Wiele P., Van Hoofl F., Bruchet A., Schmitz I., Guinumant J.L., Acobas F., Ventura A., Sacher F., Bobeldijk I., and Marecos do Monte M.H. In: Fajgelj A., and Ambrus A. (Eds). Optimization and Evaluation of Multi-Residue Methods for Priority Pesticides in Drinking and Related Waters (Principles and Practices of Method Validation) (2000), The Royal Society of Chemistry, Cambridge 9-18
40. Thompson M. Analyst 125 (2000) 385-386
41. EURACHEM Guide. In: Ellison S.L.R., Rosslein M., and Williams A. (Eds). Quantifying Uncertainty in Analytical Measurement,. first ed. (1995)
42. EURACHEM/CITAC GUIDE CG 4. In: Ellison S.L.R., Rosslein M., and Williams A. (Eds). Quantifying Uncertainty in Analytical Measurement,. second ed. (2000)
43. Nordic Committee on Food Analysis (NMKL), Estimation and expression of measurement uncertainty in chemical analysis, NMKL Secretariat, Finland procedure No. 5, second ed., 2003.
44. Hund E., Massart D.L., and Smeyers-Verbeke J. Trends Anal. Chem. 20 (2001) 394-406
45. Pecorelli I., Bibi R., Fioroni L., Piersanti A., and Galarini R. Anal. Chim. Acta A 529 (2005) 15-20