Patterning inorganic (CaCO3) thin films via a polymer-induced liquid-precursor process

Langmuir

Volumn 23, Issue 9, 2007, Pages 4862-4870

  Kim, Yi Yeoun ^a   Douglas, Elliot P ^a   Gower, Laurie B ^a  

^a University of Florida   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

COLLOIDAL DROPLETS; CONTINUOUS CALCITIC MINERAL FILMS; MICROCONTACT PRINTING TECHNIQUES; POLYMER INDUCED LIQUID PRECURSORS (PILP);

BIOMIMETIC MATERIALS; COLLOIDS; CRYSTALLIZATION; DROPS; POLYMERS; SYNTHESIS (CHEMICAL);

THIN FILMS;

CALCIUM CARBONATE; POLYMER;

ARTICLE; ARTIFICIAL MEMBRANE; CHEMISTRY; PARTICLE SIZE; SURFACE PROPERTY;

CALCIUM CARBONATE; MEMBRANES, ARTIFICIAL; PARTICLE SIZE; POLYMERS; SURFACE PROPERTIES;

EID: 34248386789     PISSN: 07437463     EISSN: None     Source Type: Journal    
DOI: 10.1021/la061975l     Document Type: Article

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78. Based on this logic, one would expect the films at the bottom of the vial to be both thicker and composed of larger particles. Unfortunately, the thickness of the films and particle size was variable across the horizontal sections of the slide. For this reason, we did not try to quantify the particle sizes. Based on visual observations of the cloudiness within the vials, vertical paths of cloudiness can be seen as the droplets tend to congregate into "streams" as they settle (note: the solution is not stirred). Pipet extractions of the streams of droplets show that they are larger the further down the vial they have traveled in the vertical section. Therefore, the observation of variable thickness across the horizontal sections is a result of the deposition of variable amounts of the droplets within streams of more concentrated regions. On the other hand, the reproducibility of increasing thickness in the vertical direction was consistent, and we therefore feel comfortable with our conclusion that the overall thickness of the films increased as the droplets settled further down the vertical height of the vial.