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The precision of this method is about ±1.5° and therefore less accurate than results obtained with the XRD method. However, the SEM images clearly show that almost all of the crystals have an orientation that fits with the 〈012〉 orientation. Only a few crystals were observed that had the 〈104〉 plane parallel to the SAM.
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This, however, would require measurements at a synchrotron facility because the diffracted signal from the SAM is very weak.
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20
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The starting pH of a crystallization solution is defined as the pH of the solution at the moment the samples are placed in the solution. The pH at which the crystallization starts is as yet unknown, but we assume that it depends on the pH value of the starting solution. Experiments regarding this issue are currently in progress and will be reported elsewhere.
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