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Crystal Growth and Design

Volumn 7, Issue 3, 2007, Pages 481-484

Layered porphyrin coordination polymers based on zinc⋯nitro recognition: Reversible intercalation of nitrobenzene

(2) Adilov, Salimgerey a Thalladi, Venkat R a

a Life Science and Bioengineering Center (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33947500344 PISSN: 15287483 EISSN: None Source Type: Journal
DOI: 10.1021/cg0607957 Document Type: Article

Times cited : (16)

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- Crystal data for 1-Zn-PhN02: C46H 30N6O4Zn·2(C6H 5NO2, M, 1042.35, monoclinic, a, 11.321(2) Å, b, 11.925(2) Å, c, 18.146-(3) Å, β, 94.312(4)°, V, 2443.0(8) Å3, T, 193 K, space group P21/c (No. 14, Z, 2, Dcalcd, 1.417 g cm-3, μ(Mo-Kα, 0.571 mm-1,4175 reflections out of 6051 unique reflections with I > 2σI, 1.80° < θ < 28.30°, final R values R1, 0.0663, wR2, 0.1506
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- 2 (65.3°) also differ significantly.

45
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- Two symmetry-independent C - H⋯O interactions (H⋯O (Å), C⋯O (Å), C-H⋯O (deg): 2.25, 3.293, 161; 2.71, 3.576, 137) and one C - H⋯π interaction (H⋯X (Å), C⋯X (Å), C-H⋯X (deg): 2.97, 3.784, 132; X refers to the centroid of aromatic rings) are seen in the crystals.
- Two symmetry-independent C - H⋯O interactions (H⋯O (Å), C⋯O (Å), C-H⋯O (deg): 2.25, 3.293, 161; 2.71, 3.576, 137) and one C - H⋯π interaction (H⋯X (Å), C⋯X (Å), C-H⋯X (deg): 2.97, 3.784, 132; X refers to the centroid of aromatic rings) are seen in the crystals.

46
- 33947491369
- It is unclear why 1-Zn shows high selectivity for the intercalation of nitrobenzene. We are currently working on the analogues of 1-Zn to test their ability toward selective inclusion of different guest species
- It is unclear why 1-Zn shows high selectivity for the intercalation of nitrobenzene. We are currently working on the analogues of 1-Zn to test their ability toward selective inclusion of different guest species.

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