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note
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-3. Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publications nos. CCDC-116979 (1), CCDC-116980 (2), and CCDC-116981 (3). Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: (+44)1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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0345240541
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note
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2 adsorption/desorption isotherm study. Further details of adsorption activity of SMTP-1 will be reported elsewhere.
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24
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0344809566
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note
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On heating by IR radiation (Mark 2 HP moisture analyzer), the guest molecules are completely removed below 200 °C: weight losses of 17.82 and 20.37% for 1 (calcd. 18.77%) and 3 (calcd. 19.65%), respectively. After loss of the solvate molecules, the open-framework structures of 1 and 3 are thermally stable up to 420 and 450 °C, respectively.
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