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Volumn 26, Issue 3, 2007, Pages 459-462

Diplatinum complexes with bridging silyl ligands. Si-H bond activation of μ-silyl ligand leading to a new platinum complex with bridging silylene and silane ligands

(3) Tanabe, Makoto a Ito, Daisuke a Osakada, Kohtaro a

a TOKYO INSTITUTE OF TECHNOLOGY (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

ACTIVATION ENERGY; COMPLEXATION; HYDROGEN BONDS; MOLECULAR STRUCTURE; PLATINUM COMPOUNDS; REACTION KINETICS; X RAY CRYSTALLOGRAPHY;

BRIDGING SILYLENE; EQUIMOLAR REACTION; SILANE LIGANDS;

SILANES;

EID: 33847199745 PISSN: 02767333 EISSN: None Source Type: Journal
DOI: 10.1021/om060930c Document Type: Article

Times cited : (38)

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- Crystallographic data for 3: C52H88P 2Si2Pt2, fw, 1221.57, triclinic, space group P1̄, a, 13.792(3) Å, b, 14.357(2) Å, c, 14.581(3) Å, α, 63.636(5)°, β= 88.025(8)°, γ, 84.744(8)°, V, 2575.8(8) Å3, Z, 2, T, 133 K, ρcalcd, 1.575 g cm-3, μ, 5.5449 mm-1, F(000, 1228, Rigaku Saturn-CCD diffractometer using graphite-monochromated Mo Ka radiation (γ, 0.71073 Å, yellow crystal (0.20 × 0.32 × 0.45 mm, Of 19314 reflections collected, 10 980 were independent (Rintm, 0.024, 609 variables refined with 8459 reflections to final R indices R1(1 > 2σ(I, 0.0644, wR2(1 > 2σ(I, 0.1383, GOF, 1.088. Crystallographic data for 4: C52H88P2Si 2Pt2, fw, 1221.57, triclinic, space group P1, a, 13.897(3) Å, b, 13.9
- int = 0.061); 604 variables refined with 5788 reflections to final R indices R1(1 > 2σ(I)) = 0.1149, wR2(I > 2σ(I)) = 0.3341, GOF = 1.118.

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