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X-ray crystallographic study of 9f: data were collected with a STOE-IPDS diffractometer using graphite-monochromated Mo Kα radiation. The structure was solved by direct methods [SIR2004: Burla, M. C, Caliandro, R, Camalli, M, Carrozzini, B, Cascarano, G. L, De Caro, L, Giacovazzo, C, Polidori, G, Spagna, R. J. Appl. Cryst. 2005, 38, 381-389] and refined by full-matrix least-squares techniques against F 2 [Sheldrick, G. M. SHELXL-97; University of Göttingen: Germany, 1997, XP (BRUKER AXS) was used for a structural representation. Space group P21/c, monoclinic, a, 13.641(3, b, 16.424(3, c, 12.005(2) Å, b, 94.29(3)°, V, 2682.1(9) Å3, Z, 4, rcalcd, 1.354 g/cm-3, 28 216 reflections measured, 4732 were independent of symmetry, of which 2669 were observed (I > 2s(I, R1, 0.042, wR2 all data, 0
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2 (all data) = 0.090, 367 parameters.
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