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Volumn 47, Issue 47, 2006, Pages 8343-8346

Pyridinium N-2′-pyridylaminide: radical cyclization in the synthesis of annulated 2-aminopyridines

Author keywords

[No Author keywords available]

Indexed keywords

AMINOPYRIDINE; PYRIDINIUM DERIVATIVE;

EID: 33749985433     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2006.09.092     Document Type: Article
Times cited : (14)

References (37)
  • 29
    • 33749985426 scopus 로고    scopus 로고
    • note
    • General procedure: A solution of TTMSS (0.248 g, 1 mmol) and AIBN (0.164 g, 1 mmol) in m-xylene (10 mL) was added dropwise by a syringe pump during 13 h to a stirred solution of the corresponding allyl derivative 10 (0.5 mmol) in m-xylene (2 mL), at 80 °C (bath temperature). Stirring was maintained at the same temperature for further 12 h. The solution was concentrated and the crude mixture was separated by flash chromatography, yielding the pure compounds (49-70%).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.