Synthesis of heterocyclic compounds using radical reactions

Tetrahedron Letters

Volumn 43, Issue 38, 2002, Pages 6865-6868

  Ganguly, A K ^a   Wang, C H ^a   David, M ^a   Bartner, P ^b   Chan, T M ^b  

^a STEVENS INSTITUTE OF TECHNOLOGY   (United States)

^b MERCK RESEARCH LABORATORIES   (United States)

Author keywords

Heterocyclic chemistry; Radical reactions

Indexed keywords

HETEROCYCLIC COMPOUND;

ARTICLE; DRUG SYNTHESIS; NUCLEAR MAGNETIC RESONANCE; OXIDATION; PROTON NUCLEAR MAGNETIC RESONANCE; RADICAL REACTION;

EID: 0037119782     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(02)01537-X     Document Type: Article

References (7)

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6. NMR and high-resolution mass spectra of all the compounds described in this communication were consistent with the assigned structures. Assignments of structures were further confirmed using HMBC and NOE experiments.
7. The percentages in parenthesis indicate yields. All the compounds described in this paper were crystalline excepting compound 4 which was an oil. The melting points of compounds 3, 5, 14, 25, 24, 28 and 32 were 133-135, 124-125, 96-98, 194-196, 197-199, 173-175 and 114-115°C, respectively. Crystals were obtained from dichloromethane and hexane.